Maize straw core absorbing material and preparing method thereof
A technology of corn stalks and adsorption materials, applied in chemical instruments and methods, and other chemical processes, can solve the problems of high pollution, low output, and unreasonable development and utilization, and achieve the effect of wide sources and simple processes
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Embodiment 1
[0022] Embodiment 1: the corn stalk cob after removing leaves and peeling off the hard shell is pulverized to 1mm, weighs 10g, mixes with the mixed solvent that the ethylene glycol of 70mL and the 35mL NaOH that mass fraction is 2% form, in autoclave Digest for 20min at a medium pressure of 0.1-0.15MPa, filter with suction, wash with ethanol with a volume concentration of 60% until neutral; 2 o 2 40mL was stirred evenly, placed in an autoclave filled with water at the bottom, steamed for 20min, cooled rapidly, and freeze-dried to obtain a fluffy white adsorption material.
Embodiment 2
[0023] Embodiment 2: the corn stalk cob after removing the leaves and peeling off the hard shell is pulverized to 2mm, weighs 10g, and is 30mL Na of 6% with the ethylene glycol of 120mL 2 CO 3 Mix the mixed solvents of the composition, cook in an autoclave for 30min under a pressure of 0.1-0.15MPa, filter with suction, wash with ethanol with a volume concentration of 70% until neutral; the obtained filter residue is washed with 5% H 2 o 2 50mL was stirred evenly, placed in an autoclave filled with water at the bottom, steamed for 30min, the water was rapidly cooled, and freeze-dried to obtain a fluffy white adsorption material.
Embodiment 3
[0024] Example 3: The corn stalk cob after the leaves and hard shells were removed was crushed to 2.8mm, 10g was weighed, and 180mL of ethylene glycol and 30mL of KHCO with a mass fraction of 10% were used 3 The mixed solvents of the composition are mixed, cooked in an autoclave under a pressure of 0.1-0.15MPa for 50min, suction filtered, and washed with ethanol with a volume concentration of 80% until neutral; the obtained filter residue is washed with 8% H 2 o 2 80mL was stirred evenly, placed in an autoclave filled with water at the bottom, steamed for 40min, cooled rapidly, and freeze-dried to obtain a fluffy white adsorption material.
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