Method for preparing flocculating agent for water treatment
A flocculant and water treatment technology, applied in the field of modified water treatment flocculant preparation, can solve the problems of application limitation, non-compliance with environmental protection requirements, and high cost of preparing polymer organic flocculants, and achieve high water solubility and viscosity stability, High water solubility, thickening, and flocculation performance are remarkable
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Embodiment 1
[0009] Take by weighing 50g of guar gum powder, simultaneously weigh 24g of monochloroacetic acid in a beaker, then add 20g of 80% ethanol to dissolve evenly, then add excessive 30g of 30% sodium hydroxide. Pour the guar gum powder into a beaker, stir at room temperature for 20 minutes, and mix well. When the material is semi-dry, crush and sieve, and remove excess ethanol if necessary. Then place the sample in a reactor beaker, heat it in a water bath to promote the reaction, control the temperature of the water bath at 60° C., and the reaction time for 1 hour. After the reaction, grind and sieve to obtain carboxymethyl guar gum.
Embodiment 2
[0011] Take by weighing 50g of guar gum powder, simultaneously weigh 35g of monochloroacetic acid in a beaker, then add 20g of 80% ethanol to dissolve evenly, then add excessive 30g of 30% sodium hydroxide. Pour the guar gum powder into a beaker, stir at room temperature for 20 minutes, and mix well. When the material is semi-dry, crush and sieve, and remove excess ethanol if necessary. Then place the sample in a reactor beaker, heat it in a water bath to promote the reaction, control the temperature of the water bath at 70° C., and the reaction time for 1 hour. After the reaction, grind and sieve to obtain carboxymethyl guar gum.
Embodiment 3
[0013] Take by weighing 36g of guar gum powder, simultaneously weigh 30g monochloroacetic acid in a beaker, then add 20g of 80% ethanol to dissolve evenly, then add excessive 30g of 30% sodium hydroxide. Pour the guar gum powder into a beaker, stir at room temperature for 20 minutes, and mix well. When the material is semi-dry, crush and sieve, and remove excess ethanol if necessary. Then place the sample in a reactor beaker, heat it in a water bath to promote the reaction, control the temperature of the water bath at 70° C., and the reaction time for 1 hour. After the reaction, grind and sieve to obtain carboxymethyl guar gum.
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