Maillard reaction product of Chinese date extract and use thereof in tobacco
A technology of reaction products and extracts, applied in the field of products and their application in tobacco, to achieve the effect of reducing harm and modifying fullness
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Embodiment 1
[0035] In a 100mL three-necked flask equipped with a thermometer, a reflux tube, and a stirring bar, add 10g jujube extract, 40mL propylene glycol aqueous solution (wherein the volume ratio of propylene glycol to water is 4:1), 5g proline, and adjust the solution with ammonia water. The pH value of the solution is 9, using ammonium dihydrogen phosphate as a catalyst, heating to 100°C within 30 minutes, and continuing the reaction for 2 hours. After cooling, a brown-red reaction product is obtained.
[0036] The "Golden Leaf" brand cigarette was used as the blank tobacco leaf, the length of the mouth rod was 20 mm, and the air permeability of the paper coil was 60 cu. Dilute the reaction product into a 10% (mass ratio) solution with 70% edible alcohol; take 50 g of flue-cured tobacco leaves, weigh the prepared alcohol solution according to 0.2% (product to tobacco weight ratio), and spray evenly on the tobacco leaves with a medical sprayer In the process, the processed samples ...
Embodiment 2-6
[0038] The time for continuing the reaction was adjusted to 0.5h, 1.0h, 1.5h, 2.5h, and 3.0h respectively. After cooling, a brown-red reaction product was obtained. Others were the same as in Example 1. The perfuming effects were shown in Table 1.
[0039] Table 1
[0040]
Embodiment 7-9
[0042] The pH values of the adjustment system were 7, 8, and 10 respectively, and the others were the same as in Example 1. The results of perfuming are shown in Table 2.
[0043] Table 2
[0044]
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