High-temperature and high-pressure hydrogenation method for castor oil
A high temperature and high pressure, castor oil technology, applied in the direction of fatty acid hydrogenation, etc., can solve the problems of unstable product quality, waste of production cost, low equipment utilization rate, etc., to shorten the hydrogenation reaction time, reduce equipment loss, and improve production efficiency. Effect
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Embodiment 1
[0011] Pump the refined castor oil heated to 100°C into the hydrogenation reactor, vacuumize the reactor with vacuum equipment and heat it to 125°C, dehydrate the castor oil in the reactor, and then add nickel hydrogenation catalyst , the amount of catalyst added is 0.9‰ of the weight of castor oil, hydrogen is passed into the reactor, and the amount of hydrogen that is passed into is 65m per ton of castor oil 3 , the pressure in the reactor is 2Mpa, and the temperature is 130°C. After 7 hours of hydrogenation reaction, unreacted hydrogen is discharged, and then the catalyst in the hydrogenated castor oil is removed by filtration to obtain hydrogenated castor oil.
Embodiment 2
[0013] Pump the refined castor oil heated to 110°C into the hydrogenation reactor, vacuumize the reactor with vacuum equipment and heat it to 135°C, dehydrate the castor oil in the reactor, and then add nickel hydrogenation catalyst , the amount of catalyst added is 1.1‰ of the weight of castor oil, hydrogen is passed into the reactor, and the amount of hydrogen passed into is 80m per ton of castor oil 3 , the pressure in the reactor is 2.5Mpa, and the temperature is 150°C. After 5 hours of hydrogenation reaction, unreacted hydrogen is discharged, and then the catalyst in the hydrogenated castor oil is removed by filtration to obtain hydrogenated castor oil.
Embodiment 3
[0015] Add 9901 nickel hydrogenation catalyst in the reaction kettle with refined castor oil, the amount of catalyst added is 1.0‰ of castor oil weight, then feed hydrogen into the reaction kettle, the amount of hydrogen is 75m per ton of castor oil 3 , the pressure in the reactor is 2.3Mpa, and the temperature is 140°C. After 6 hours of hydrogenation reaction, unreacted hydrogen is discharged, and then filtered to remove the catalyst in the hydrogenated castor oil to obtain hydrogenated castor oil.
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