Lock color method for phenols products
A product and color stabilization technology, applied in chemical instruments and methods, preparation of organic compounds, organic chemistry, etc., can solve problems such as color stabilization methods that have not yet been found, and achieve continuous and stable appearance and color, commercial value expansion, environmental protection and rational utilization The effect of resources
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[0015] The following examples describe the present invention in more detail:
[0016] (1) Extraction process
[0017] The crude phenol is vacuum sucked into the heating kettle of the rectification system for distillation, and the fractions of cresol, m-p-cresol and xylenol are cut. Pour the distillate into the extraction tank and add the extraction agent 85% industrial phosphoric acid. The phenol fraction and the extraction agent are mixed according to the ratio of 6.5-26.5:1 (W / W). 1.5 hours, stand still for 2-4 hours, when the phase interface in the extraction kettle is stable, the upper layer is the phenol fraction, the lower layer is the extractant, and the extractant residue is discharged, and the extracted cresol and m-p-cresol are left in the extraction kettle , Xylenol fraction.
[0018] (2) Adsorption process
[0019] Heat the extracted cresol, m-p-cresol and xylenol fractions to 105-130°C and pour them into the adsorption kettle, then add the adsorbent industrial ...
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