Preparing process for extracting inulin from chicory root

A preparation process and a technology for chicory, which are applied in the field of chemical extraction process and the preparation process for extracting inulin from chicory roots, can solve the problems of low purity and yield of inulin, complicated process, long extraction time and the like, and achieve high purity and yield, The effect of easy availability of raw materials and short extraction time

Inactive Publication Date: 2007-08-08
鞍山市维康生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The present invention aims at the problems existing in the above-mentioned prior art, according to the modern extraction theory, carries out a large amount of groping and test summary, develops a kind of preparation technology of extracting

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] Extraction process of the present invention comprises the following steps:

[0025] Cleaning: remove impurities from the chicory rhizomes and wash them with water;

[0026] Slicing: Cut the cleaned chicory rhizomes into slices;

[0027] Drying and pulverizing: drying the chicory rhizome processed into slices for 2 hours, controlling the temperature at 80° C., and pulverizing to obtain pulverized chicory rhizome A;

[0028] Extraction and filtration: the pulverized chicory rhizome A is reflux extracted 3 times with 50% ethanol, the amount of ethanol is 8 times, 6 times and 6 times of the weight of raw material A respectively, and the extraction time is 2 hours, 1 hour and 1 hour respectively, and combined The extract was filtered to obtain filtrate B;

[0029] Heating to reflux: add decolorizing agent magnesium oxide according to 5% of the volume of filtrate B, heat to reflux for 3 hours, filter to obtain filtrate C;

[0030] Concentration and drying: Concentrate the ...

Embodiment 2

[0032] In the dry crushing step, dry for 0.5 hours, and the temperature is controlled at 50°C; in the extraction and filtration step, use 10% ethanol to reflux and extract once, the amount of ethanol is twice the weight of raw material A, and the extraction time is 0.5 hours; heat to reflux In the step, add the decolorizing agent aluminum oxide according to 0.1% of the volume of the filtrate B, and heat and reflux for 0.1 hour; in the concentration and drying step, concentrate under reduced pressure at 1 mm Hg, dry in vacuum, and control the water content to 2%, and the others are the same as in the embodiment 1.

Embodiment 3

[0034] In the dry crushing step, dry for 10 hours, and the temperature is controlled at 100°C; in the extraction and filtration step, reflux extraction with 95% ethanol for 5 times, the amount of ethanol each time is 15 times the weight of raw material A, and the extraction time is 5 hours ; In the heating and reflux step, add the decolorant activated carbon according to 50% of the volume of the filtrate B, and heat and reflux for 10 hours; Step is with embodiment 1.

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PUM

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Abstract

The invention discloses an extracting method of inulin from chicory root, which comprises the following steps: cleaning; cutting; drying at 50-100 deg.c for 0.5-10h; grinding; extracting through 10-95% alcohol for 1-5 times; setting each extracting time for 0.5-5h; combining extract; filtering; obtaining filtrate B; adding 0.1-50% decolourant corresponding to filtrate B; heating to reflux 0.1-10h; filtering; obtaining the filtrate C; decompressing the filtrate C under 1-760 mm mercury column; condensing; drying in the vacuum; controlling water content at 2-10%.

Description

technical field [0001] The invention relates to a plant extraction process, in particular to a preparation process for extracting inulin from chicory roots, which belongs to the chemical extraction process. Background technique [0002] Chicory (also known as European Chicory) is a perennial herb of Compositae, native to Europe, and widely used as raw material for feed and vegetable sugar production abroad. After the introduction in my country in the 1980s, a large-leaf variety was cultivated. Because of its excellent quality, it has become the most promising new breed of feed and economic crops. [0003] Chicory has a wide range of uses. For example, it is used in aquaculture. Because of its excellent palatability, all poultry and grass carp love to eat it. It is a high-quality green fodder; High-quality edible mushroom base material; rich inulin and spices can be extracted from the rhizome. [0004] Modern studies have proved that chicory extract can significantly reduce...

Claims

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Application Information

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IPC IPC(8): C08B37/00
Inventor 王庆君江敦化
Owner 鞍山市维康生物科技有限公司
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