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Long lasting waterproof sunscreen comprising metal oxide and peptide conditioner

a technology of peptide conditioner and sunscreen, which is applied in the direction of peptide/protein ingredients, peptide sources, hair cosmetics, etc., can solve the problems of lack of durability for long-lasting effects, and achieve high chemical stability, reduce the tendency to form agglomerates, and high photo stability

Inactive Publication Date: 2007-11-29
DUPONT US HLDG LLC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

[0020] Typically, the metal oxide prepared by this process is titanium dioxide, especially titanium dioxide nanoparticles. The metal oxide particles prepared by this process have been found to have a high photo stability and / or high chemical stability. In addition the nanoparticles have a reduced tendency to form agglomerates when formulated into sunscreen composition.

Problems solved by technology

A major problem with current skin care compositions is that they lack the required durability for long-lasting effects.

Method used

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  • Long lasting waterproof sunscreen comprising metal oxide and peptide conditioner
  • Long lasting waterproof sunscreen comprising metal oxide and peptide conditioner

Examples

Experimental program
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Effect test

example 1

[0133] In a half gallon plastic jug containing 100 g titanium dioxide nanoparticles made by RF plasma oxidation according to U.S. 2002 / 0155059A1, 800 mls. total volume deionized polished water was added and the mixture was stirred. The titanium dioxide nanoparticles starting material had a mean particle size of 90 nm, 10 wt % of particles less than 50 nm in size, and 90% of particles less than 150 nm in size as measured by the Microtrac UPA dynamic light scattering instrument. The mixture was sonicated for 10 minutes at a power of 7 and screened through a 325 mesh sieve. The screened mixture was added to a 2000 ml stainless steel beaker equipped with an electric stirrer, temperature probe and pH probe. The mixture was rapidly stirred using a propeller blade.

[0134] The initial pH was 1. The mixture was heated to 60° C. and the pH was adjusted to 7.1 with 50% NaOH solution (8.2 g). Then 9.0 g sodium aluminate (27.8 wt % alumina) was added. The pH was 10.8. The mixture was stirred for...

example 2

[0138] The following materials were added to a 1000 ml plastic beaker: 50.00 g Degussa P25 titanium and 400 ml deionized polished water. The mixture was stirred then sonicated for 3 minutes at a power of 7. The mixture was then poured into a 600 ml stainless steel beaker equipped with an electric stirrer, temperature probe and pH probe. The mixture was agitated using a propeller blade. The initial pH of the mixture was 3.3. The mixture was heated to about 95° C. and 0.8 g citric acid 50% solution was added. The pH was 2.7. The pH was adjusted with 10% NaOH to a range of 9-9.5 by adding 3.8 g 50% NaOH solution. The neutral pH was maintained by adding 8.1 g concentrated (38%) HCl while adding 10.75 g sodium silicate drop wise over 14 minutes. The mixture was heated at 95° C. for one hour at pH 9.5 with stirring at about 2600 rpm. The pH was lowered to 7 by adding 8.1 g concentrated (38%) HCl while 9 g sodium aluminate was added drop wise over 10 minutes. The heat was turned off and th...

example 3

[0142] The treatment was performed as in Example 1 except no sodium aluminate was added prior to the addition of sodium silicate. [0143] Measured SiO2: 4.1% [0144] Measured Al2O3: 4.4%

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Abstract

The disclosure provides a sunscreen formulation comprising a peptide-based metal oxide sunscreen agent, such as titanium dioxide nanoparticles, and a fluid vehicle.

Description

CROSS-REFERENCE TO RELATED APPLICATIONS [0001] This application is a continuation-in-part of application Ser. No. 11 / 011,670 filed on Dec. 14, 2004 which is a continuation-in-part of application Ser. No. 10 / 737,357, filed Dec. 16, 2003 which are both incorporated herein by reference in their entireties. [0002] This application is a continuation-in-part of application Ser. No. 10 / 935,642 filed on Sep. 7, 2004 which is incorporated herein by reference in its entirety.FIELD OF THE INVENTION [0003] The present invention relates to sunscreen compositions. More specifically, the invention relates to sunscreen screen compositions based upon inorganic metal oxides and skin-binding, peptides. BACKGROUND OF THE INVENTION [0004] Certain metal oxides, such as titanium dioxide and zinc oxide, are known for their sunscreen properties. Titanium dioxide has low toxicity and is non-irritating to the skin. [0005] Nanostructured particles and materials are currently attracting considerable attention. ...

Claims

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Application Information

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Patent Type & Authority Applications(United States)
IPC IPC(8): A61K7/42C07K14/47A61K38/08A61K8/29A61K8/64A61Q1/10A61Q5/06A61Q5/12A61Q11/00A61Q17/04
CPCA61K8/19Y10S977/836A61K8/29A61K8/64A61K38/08A61K38/10A61K47/48238A61K47/48861A61K47/48884A61K2800/413A61K2800/57A61K2800/94A61Q1/10A61Q5/065A61Q5/12A61Q11/00A61Q17/04B82Y5/00Y10S977/926A61K8/27A61K47/62A61K47/6923A61K47/6929A61P17/16
Inventor BUSEMAN-WILLIAMS, JANINEHUANG, XUEYINGWANG, HONGWHITING, GARY KEN
Owner DUPONT US HLDG LLC
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