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Bonded magnets made with atomized permanent magnetic powders

A magnetic powder and magnet technology, applied in the direction of magnetic objects, magnetic materials, inorganic materials, etc., can solve the problems of magnet cracking, internal coercive force loss, high magnetic flux loss, etc., and achieve small internal magnetic shear loss and magnetic flux loss. Small, small coercivity loss effect

Inactive Publication Date: 2005-03-09
MAGNEQUENCH INT INC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Benefits of technology

This patented inventor describes an improvement on traditional permanent magnets that use iron oxide (Fe2O3). These improvements include reduced losses caused during repetitive casting processes due to large external forces applied thereto, increased stability when exposed to heat over time, less susceptibility towards chemical reactions compared to other materials used for making them, lower levels of electrical resistance at room temperatures, better flowability than liquid binder mixtures, and greater structural rigidness without compromising their effectiveness.

Problems solved by technology

This technical problem addressed in this patents relates to improving the efficiency of making strong magnets while maintaining desired levels of intrinsic intensity without losing magneque stability when exposed to external environments like airborne dustors or moisture sources over time. Existing techniques involve injectable binders, including metal alloys containing iron cations, dendritisferriphilites, amorphous rare earth materials, etc., which may lead to reduced quality of magnet cores and decreased durability under harsh conditions.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0059] The alloy whose nominal composition is 19% Nd; 2% 5Ti; 4% Zr; 1.6% B; the rest is Fe powder is made into powder by centrifugal atomization method, and the rotation speed of the rotating disc is about 30,000rpm, and the obtained isotropic Isotropic powders are cooled in a helium atmosphere. The powder thus obtained is substantially spherical. The average particle size of the powder is about 55 μm. After a suitable heat treatment, the powder is mixed with polyamide analogously to comparative product 1 . The preparation of the bonded magnet was as in Comparative Product 1. The test was carried out similarly to comparative product 1, determining the loss of internal coercive force. The measured values ​​are also shown in Table 1.

[0060] As shown in Table 1, the internal coercivity loss of the bonded magnet of the present invention is lower than 5% (as shown in Example 1), which is 22% compared with that of the conventional magnet (represented by Comparative Product 1)...

Embodiment 2

[0065] In this example, the bonded magnet was prepared using the composition of the atomized magnetic powder given in Example 1. The magnetic powder content of Comparative Product 2 was varied from 20% to 80% by volume. The internal loss of each constant volume loading was measured and shown in Table 2, Example 2.

[0066] Table 2 shows the internal losses of bonded magnets prepared using melt-spinning and atomized magnetic powders. When using the atomized magnetic powder of the present invention (Table 2, Example 2), the bonded magnets had lower internal losses and thus improved magnetic performance at various magnetic powder loading levels.

[0067] Compare product 3

[0068] An alloy with a nominal composition of 20% Nd, 6.5% Pr, 1.3% B, 0.08% Cu, balance Fe was melt-spun and then annealed. The obtained isotropic powder was pulverized to a particle size of about 150 μm, and a bonded magnet was prepared by injection molding. Different amounts of magnetic powder and pol...

Embodiment 3

[0070] The alloy of the composition given in Example 1 was atomized as described in Example 1 by centrifugal atomization. The average particle size of the magnetic powder is about 55 μm. After heat treatment, magnetic powder was mixed with polyamide binder as in comparative product 3 to obtain constant volume loading of magnetic material of 63%, 67% and 69%. The composite composition of atomized magnetic powder up to 72vol% can be used to produce injection molded magnets. There are no cracks or deformations in this magnet. The improvement in magnetic properties (Br in this example) due to the increase in the constant volume loading of the magnetic material is shown in Table 3.

[0071] Loading capacity of magnetic material

(volume%)

Compare product 3

Magnet Br (thousand Gauss)

Example 3

Magnet Br (thousand Gauss)

63

5.05

4.68

67

cannot produce

5.00

69

cannot p...

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Abstract

The invention relates to magnets, particularly bonded magnets, of the Re-Fe-B type made from atomized magnetic powders and to methods of producing the powders and the magnet. The magnetic powders comprise, by weight, about 15 % to 25 % of RE; about 0.8 % to 2.0 % of B; about 1 % to 10 % of T; and balanced with Fe, Co, or mixtures thereof; wherein RE is one or more rare earth elements selected from the group consisting of Y, La, Ce, Pr, Nd, Sm, Er, Gd, Tb, Dy, Ho, Tm, Yb and Lu, and T is one or more elements selected from the group consisting of Ti, Zr, Hf, V, Nb, Ta, Cr, Mo and W. To produce bonded magnets, the atomized powders are heat treated, combined with a binder, pressed or molded, and cured to produce the bonded magnets. As compared to bonded magnets made from melt-spun powders or from other conventional atomized powders, bonded magnets of the present invention exhibit one or more of the following properties: less loss of intrinsic coercivity under repeated injection molding cycles; less internal magnetic shearing loss; improved flowability of the magnetic powders; improved Br and part integrity; less environmental degradation after exposure to high temperature and less flux loss; complex shapes and high part integrity; lower viscosity of the magnetic powder-binder mixtures; and high magnetic strength even for small-dimension magnets.

Description

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Claims

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Application Information

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Owner MAGNEQUENCH INT INC
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