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Evaluation method for nano powder material light catalysis property

A nano-powder, photocatalytic technology, applied in the direction of chemical analysis using catalysis, can solve expensive, such as scanning tunneling microscope, atomic force microscope, laser detection atomic force microscope, low temperature scanning microscope, vacuum scanning tunneling One hundred thousand yuan or even several million yuan, can not be determined and other problems, to achieve the effect of fast analysis and testing, simple equipment, and low cost

Inactive Publication Date: 2003-04-09
EAST CHINA NORMAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In order to identify and inspect nanopowder materials and observe their surface properties, a series of nanopowder material characterization methods have been developed, but the instruments used in these methods are very expensive, such as scanning tunneling microscope, atomic force microscope, laser detection atomic force microscope, cryogenic scanning Microscopes, vacuum scanning tunneling microscopes, ballistic electron emission microscopes, etc., the price of a stand-alone machine is hundreds of thousands or even millions of yuan, which greatly limits the application of these methods
In addition, these methods can only provide limited structural information such as material size, surface morphology, and crystal form, while properties such as chemical properties that are closely related to the practical application of nanopowder materials cannot be determined.

Method used

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  • Evaluation method for nano powder material light catalysis property
  • Evaluation method for nano powder material light catalysis property
  • Evaluation method for nano powder material light catalysis property

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] The nano powder material to be evaluated is P25 nano TiO produced by Germany Degussa company 2 Material. Its specific technical indicators are: particle size: 30nm; crystal form: 80% anatase phase, 20% rutile phase; preparation method: gas phase method. Utilize the photocatalytic performance evaluation method of the nano powder material provided by the present invention to carry out the photocatalytic performance evaluation, record the final absorbance A of the methyl orange solution at a wavelength of 470nm T 0.314, less than 0.5, the photocatalytic performance of the nano powder material is superior. It shows that the nano-powder material has good photocatalytic performance and can be used in the field of environmental optimization such as industrial sewage treatment, sterilization and disinfection.

Embodiment 2

[0040] The nano powder material to be evaluated is self-made HSD-2001 nano TiO 2 Sample after material treatment at 500°C for 3 hours. Utilize the photocatalytic performance evaluation method of the nano powder material provided by the present invention to carry out the photocatalytic performance evaluation, record the final absorbance A of the methyl orange solution at a wavelength of 470nm T It is 0.910, between 0.5 and 1.0, and the photocatalytic performance of the nanopowder material belongs to the passing grade.

Embodiment 3

[0042] The nano powder material to be evaluated is 101nm TiO specially used for coatings 2 . Utilize the photocatalytic performance evaluation method of the nano powder material provided by the present invention to carry out the photocatalytic performance evaluation, record the final absorbance A of the methyl orange solution at a wavelength of 470nm T is 1.161, and greater than 1.0, the photocatalytic performance of the nanopowder material is at a poor level, and the photocatalytic activity is relatively poor.

[0043] The above examples illustrate that the method for evaluating the photocatalytic performance of the nano-powder material provided by the present invention has various meanings: at first, utilizing the present invention and the evaluation criteria provided therefor, to regulate the nano-powder material market, effectively and effectively Secondly, from a specific aspect, the present invention and the standards provided by it can provide a specific basis for the ...

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Abstract

A photocatalysis performance estimating method for nano powder material, belonging to the estimating technical field of material chemical properties, includes seven steps in operation as setting up aphotocatalysis device, preparing a photocatalysis degradation solution, degradation reaction of photocatalysis, centrifugal ization, taking the solution, determining the unabsorbance Ar, and estimating the grade of photocatlaysis performance of the nano powder material. Through making the estimated standard of photocatalysis, the quality grade for photocatalyst of the nano powder material can be determined and it provides the direct basis for the use of nanopowder material. The method only uses very simple instrument, but also is quick in detection so that it has a very good prospect for the application to environmental protection and food freshness-keeping field of nano powder material.

Description

Technical field [0001] The invention relates to a method for evaluating the photocatalytic performance of a nano-powder material, which belongs to the technical field of material chemical property evaluation. Background technique [0002] Nanotechnology is a high-tech that was born in the late 1980s and is developing vigorously. As one of its products, nanopowder materials embody modern technologies such as small size, complex structure, high integration, strong interaction and high specific surface area. specialty. At the nanometer size, the material has many specific properties that conventional materials do not have, such as: quantum effect, surface effect, volume effect, etc., and its optical, thermal, electrical, magnetic, mechanical and especially some chemical properties have also occurred. These changes have contributed to the research and application of nano-powder materials in many fields. In order to identify and inspect nanopowder materials ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N31/10
Inventor 金利通陈俊水刘梅川鲜跃仲朱民张文张莉张继东
Owner EAST CHINA NORMAL UNIV
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