A method for controlling the mechanical properties of nial-based composites through powder particle size refinement
A technology of fine control and composite materials, applied in transportation and packaging, metal processing equipment, etc., which can solve the problems of difficult fine control of grain size, difficult coordination of room temperature toughness and high temperature strength, etc.
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specific Embodiment approach 1
[0041] Embodiment 1: A method for controlling the mechanical properties of NiAl-based composite materials through powder particle size refinement in this embodiment is completed by the following steps:
[0042] 1. Sieve the NiAl-based composite alloy powder into 5 groups of original powders with different average particle sizes;
[0043] The average particle sizes of the 5 groups of original powders in step 1 are 10 μm, 20 μm, 30 μm, 40 μm and 50 μm respectively;
[0044] 2. Put 5 groups of original powders with different average particle diameters into 5 mixing buckets, respectively, and fill the 5 mixing buckets with O 2 , and then put the 5 mixing buckets on the drum ball mill to mix the powder, and obtain 5 groups of surface fully adhered O 2 alloy powder;
[0045] 3. Transfer the 5 sets of gold powders into 5 molds respectively, apply pressure and maintain the pressure respectively, and then put the 5 molds into the spark plasma sintering furnace respectively;
[0046]...
specific Embodiment approach 2
[0067] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the preparation method of the NiAl-based composite material alloy powder described in Step 1 is as follows:
[0068] 1. Weigh metal Ni particles, Al particles and Hf particles, mix them evenly, and then vacuum refining twice at a temperature of 1500 °C, and the time of each vacuum refining is 5 minutes to obtain a liquid alloy;
[0069] 2. Transfer the liquid alloy into a cylindrical mold for cooling to obtain a cylindrical cast alloy;
[0070] 3. The cylindrical as-cast alloy is prepared into NiAl-based composite material alloy powder by argon atomization method. Other steps are the same as in the first embodiment.
specific Embodiment approach 3
[0071] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the purity of the metal Ni particles, Al particles and Hf particles described in Step 1 is greater than 99.5%. Other steps are the same as in the first or second embodiment.
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