Homogeneous C and N co-doped phosphate material as well as preparation method and application thereof
A phosphate and co-doping technology, applied in chemical instruments and methods, phosphorus compounds, hybrid/electric double layer capacitor manufacturing, etc., can solve the problems of large mass transfer resistance, high overpotential, etc., and achieve small size and high conductivity High and simple preparation method
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[0030] The main raw materials used in Examples 1 to 10 of the present invention and their consumption and reaction conditions are shown in Table 1 below:
[0031] Table 1
[0032]
[0033] A kind of homogeneous C of embodiment 1~10 of the present invention, the preparation method of N co-doped phosphate material comprises the following steps:
[0034] According to the ratio and reaction conditions shown in Table 1, after mixing the cobalt source, phosphoric acid, and solvent, adding an organic amine to obtain a gel, the gel is transferred to a high-pressure tube for reaction, and the obtained product is washed with water or ethanol at least three times, and dried After drying, the 2D phosphates of Examples 1-10 were obtained, denoted as CxNCPO.
[0035] It should be noted that x in CxNCPO is 3, 4 or 6; when x is 3, it shows that the prepared 2D phosphate (C3NCPO) is a 2D structure with 1,3-propanediamine intercalated between layers; When x is 4, it shows that the prepared...
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