A device for separating and purifying traditional Chinese medicine components by alcohol precipitation tank, its method and application

A technology of alcohol precipitation tank and traditional Chinese medicine, applied in separation methods, chemical instruments and methods, solid solvent extraction, etc., can solve problems such as long alcohol precipitation time, clogging of filters or filter meshes, and affecting production efficiency, so as to reduce alcohol The effect of sinking time and avoiding clogging pipes

Active Publication Date: 2022-06-21
SHANDONG MINGREN FURUIDA PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] However, the inventors have found that although the existing methods can remove impurities in traditional Chinese medicine components, the alcohol precipitation time is too long, which affects production efficiency
If the alcohol precipitation time is simply shortened, the solution discharged through the drain pipe cannot remove residual impurities or particles, which will not only affect the quality of the alcohol precipitation solution, but also cause certain damage to the density meter
Although some technologies regulate the purity of the outlet liquid through auxiliary devices (filters or filter screens), the filter or filter screen holes are prone to clogging, and the supernatant liquid after alcohol precipitation has a high viscosity, and it is difficult to pass through a fine-meshed filter screen. Larger, requires a larger vacuum pump to provide power, consumes a lot of energy, and has low production efficiency

Method used

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  • A device for separating and purifying traditional Chinese medicine components by alcohol precipitation tank, its method and application
  • A device for separating and purifying traditional Chinese medicine components by alcohol precipitation tank, its method and application
  • A device for separating and purifying traditional Chinese medicine components by alcohol precipitation tank, its method and application

Examples

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Effect test

Embodiment 1

[0047] like figure 1 As shown, a device for separating and purifying traditional Chinese medicine components in an alcohol precipitation tank provided in this embodiment includes an alcohol precipitation tank 1, and the alcohol precipitation tank 1 is provided with a feed port 2, a stirrer 3 and a discharge line 4, and the The material pipeline 4 is connected to the serpentine pipe 5, the density meter 6 is connected to the discharge pipeline 4 through the serpentine pipe 5, and a vacuum pump 7 is provided at the end of the density meter 6 away from the alcohol precipitation tank 1.

[0048] like figure 2 As shown, it is an enlarged view of the serpentine tube 5. The serpentine tube 5 is sequentially connected by a first straight tube 8 and a first elbow 9. The first elbow 9 is arc-shaped and is tangentially connected to the first straight tube 8 , the first straight pipe 8 and the first curved pipe 9 are detachably connected, and the first straight pipe 8 is arranged horizo...

Embodiment 2

[0054] like image 3 As shown, another device for separating and purifying traditional Chinese medicine components provided by an alcohol precipitation tank in this embodiment is different from Embodiment 1 in that the first straight pipe 8 is arranged vertically.

Embodiment 3

[0056] like Figure 4 As shown, the device of another kind of alcohol precipitation tank separation and purification of traditional Chinese medicine composition provided in this embodiment is different from embodiment 1 in that the serpentine tube adopts the method of two-layer casing, and the first straight tube 8 and the second straight tube are set. Pipe 11, first elbow 9, second elbow 12, the first straight pipe 8 is connected to the first elbow 9, the second straight pipe 11 is connected to the second elbow 12, and the first straight pipe 8 is arranged on the second On the periphery of the straight pipe 11, the two are coaxially arranged, the diameter of the first straight pipe 8 is larger than that of the second straight pipe 11, and the first curved pipe 9 is arranged on the periphery of the second curved pipe 12. The diameter of the second elbow 12 . On the outer wall of the second elbow 12 , a baffle 10 is arranged between the inner wall of the first elbow 9 , the in...

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Abstract

The invention relates to the field of medicine production devices, in particular to a device for separating and purifying traditional Chinese medicine components in an alcohol precipitation tank, as well as its method and application. In order to solve the problems of uneven supernatant and incomplete removal of impurities in the prior art, the present invention proposes a device for separating and purifying Chinese medicine components in an alcohol precipitation tank and its method and application. By designing a serpentine tube in front of the density meter, When the precipitation supernatant flows through the serpentine pipe, the direction of the bend in the pipe changes abruptly, so that the solution is mixed evenly, which helps to improve the accuracy of the density meter detection. At the same time, due to a certain centrifugal effect at the elbow, the impurities have greater inertia than the solution and move downward against the outer wall of the elbow. At this time, a baffle is designed at the end of the elbow to help intercept impurities. At the same time, due to the blocking effect of the baffle, it cooperates with the elbow to realize further mixing of the liquid and improve the detection accuracy.

Description

technical field [0001] The invention relates to the field of pharmaceutical production devices, in particular to a device for separating and purifying traditional Chinese medicine components in an alcohol precipitation tank, a method and application thereof. Background technique [0002] The disclosure of information in this Background section is only for enhancement of understanding of the general background of the invention and should not necessarily be taken as an acknowledgement or any form of suggestion that this information forms the prior art already known to a person of ordinary skill in the art. [0003] In the alcohol precipitation process in the production process of traditional Chinese medicine, ethanol is mainly introduced into the extract at room temperature or low temperature for precipitation, and a large amount of high-concentration ethanol is added at the beginning of alcohol precipitation. If the alcohol content is too high, starch and proteins will rapidl...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D11/02
CPCB01D11/0288
Inventor 贾美春毋立华林志展赵晓辉刘大勇寇杰邱烜韩苗苗
Owner SHANDONG MINGREN FURUIDA PHARMA
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