A kind of quartz fiber reinforced quartz-based composite material and its manufacturing method
A composite material and quartz fiber technology, which is applied in the field of high-temperature-resistant wave-transparent composite material preparation, achieves the effects of simple equipment, wide range of raw materials, and improved densification efficiency
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Embodiment 1
[0041] A method for manufacturing a quartz fiber reinforced quartz-based composite material, comprising the following steps:
[0042] 1) Preparation of fiber prefabricated parts: Quartz fiber slabs are prepared as prefabricated parts by 2.5D weaving method, the fiber volume fraction is 35%, and the length, width and height are 100mm×100mm×20mm; SiO 2f / SiO 2 The density of the composite material flat plate is required to be 1.65g / cm 3 ;
[0043] Soak the quartz fiber preform in acetone for 10 hours each time, and then dry it in an oven at 100°C for 2 hours to remove the wetting agent and impurities on the surface of the fiber. Repeat "soaking-drying" 3 times, each time Soak and replace with new acetone;
[0044] 2) Pour 2 kg of commercially available acidic silica sol with a solid content of 25%, pH = 2, and a viscosity of less than 10 mPa·s into the flask matched with the rotary evaporator, connect the flask to the rotary evaporator, and evacuate to 6×10 -2 MPa, check the...
Embodiment 2
[0052] A method for manufacturing a quartz fiber reinforced quartz-based composite material, comprising the following steps:
[0053] 1) Preparation of fiber preforms:
[0054] The quartz fiber plate is prepared as a prefabricated part by laying up and suturing, the fiber volume fraction is 50%, and the length, width and height are 100mm×100mm×20mm; SiO 2f / SiO 2 The density of the composite material flat plate is required to be 1.75g / cm 3 ;
[0055] Soak the quartz fiber preform in acetone for 10 hours each time, and then dry it in an oven at 100°C for 2 hours to remove the wetting agent and impurities on the surface of the fiber. Repeat "soaking-drying" 3 times, each time Soak and replace with new acetone;
[0056] 2) Pour 2kg of commercially available acidic silica sol with a solid content of 20%, pH = 4, and a viscosity of less than 10mPa·s into the flask matched with the rotary evaporator, connect the flask to the rotary evaporator, and evacuate to 6×10 -2 MPa, check...
Embodiment 3
[0064] A method for manufacturing a quartz fiber reinforced quartz-based composite material, comprising the following steps:
[0065] 1) Preparation of fiber prefabricated parts: Quartz fiber slabs were prepared as prefabricated parts by 2D puncture, the fiber volume fraction was 45%, and the length, width and height were 100mm×100mm×20mm; SiO 2f / SiO 2 The density requirement of the composite plate is 1.70g / cm 3 ;
[0066] Soak the quartz fiber preform in acetone for 10 hours each time, and then dry it in an oven at 100°C for 2 hours to remove the wetting agent and impurities on the surface of the fiber. Repeat "soaking-drying" 3 times, each time Soak and replace with new acetone;
[0067] 2) Pour 2 kg of commercially available acidic silica sol with a solid content of 23%, pH = 3, and a viscosity of less than 10 mPa·s into the flask matched with the rotary evaporator, connect the flask to the rotary evaporator, and evacuate to 6×10 -2 MPa, check the air tightness, under ...
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