Aluminum silicon carbide material and preparation method thereof
A technology of aluminum silicon carbide and silicon carbide, which is applied in the field of aluminum silicon carbide materials and its preparation, can solve the problems of low thermal conductivity of aluminum silicon carbide materials, low strength of silicon carbide prefabricated parts, and difficulty in meeting electronic packaging, so as to improve the strength , Reduce the formation of silica, improve the effect of thermal conductivity
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[0021] The present invention also provides a method for preparing an aluminum silicon carbide material, the preparation method comprising the following steps:
[0022] S1. Mix 100 parts by weight of silicon carbide particles, 1-10 parts by weight of metal nitrate and 1-10 parts by weight of binder to obtain a mixture;
[0023] S2. Drying and molding the mixed material to obtain a green body;
[0024] S3. Sintering the green body to obtain a silicon carbide preform;
[0025] S4. Perform aluminizing treatment on the silicon carbide preform to obtain an aluminum silicon carbide material.
[0026] In the present invention, preferably, the silicon carbide particles in the step S1 include coarse silicon carbide particles and fine silicon carbide particles; the D50 of the coarse silicon carbide particles is 90-150 μm, and the D50 of the fine silicon carbide particles is 10-20μm. Preferably, the coarse silicon carbide particles are mixed with the fine silicon carbide particles in a...
Embodiment 1
[0035] The preparation method of the aluminum silicon carbide material of the present embodiment is:
[0036] (1) Mix 100 parts by weight of coarse silicon carbide particles (D50=146μm) and fine silicon carbide particles (D50=16μm) at a weight ratio of 2:1, then add 1 part by weight of aluminum nitrate aqueous solution and 2 The ethanol solution of the phenolic resin in parts by weight is continuously mixed to obtain a mixture.
[0037] (2) Dry the mixture at 80°C for 1 hour. After it is cooled to room temperature, it is granulated through a granulator through an 80-mesh sieve to obtain pellets. The humidity is controlled at 2%.
[0038] (3) Fill the pellets into a steel mold, and shape it under a pressure of 18 MPa for 30 seconds to obtain a green body.
[0039](4) Curing the green body at 200°C for 4h.
[0040] (5) Sinter the cured green body at 1200°C for 2 hours to obtain the silicon carbide preform S01.
[0041] (6) Put the silicon carbide preform S01 into a graphite m...
Embodiment 2
[0043] The preparation method of the aluminum silicon carbide material of this example is the same as that of Example 1, except that 5 parts by weight of an aqueous solution of aluminum nitrate and 3 parts by weight of an ethanol solution of phenolic resin are added in step (1). An aluminum silicon carbide material S2 is also obtained.
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