A kind of heavy metal polluted soil remediation method
A technology of polluted soil and remediation method, applied in the field of heavy metal contaminated soil remediation, can solve the problems of complicated operation steps, large energy consumption, etc., and achieve the effects of large specific surface area, increased soil organic carbon content, and strong adsorption capacity
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Embodiment 1
[0047] A preparation method of modified magnetic biochar, comprising the steps of:
[0048] (1) After crushing 50g of peanut shell biochar raw material to a particle size of 2-5mm, soak it in 1L 50mM FeSO 4 . 7H 2 O solution, shake at room temperature for 12h and filter to obtain solid raw material;
[0049] (2) drying the solid raw material obtained in step (1) at 60°C, and then pyrolyzing it at 600°C for 1.5 hours to obtain magnetic biochar;
[0050] (3) Prepare magnetic biochar-supported Ca-Al hydrotalcite adsorbent by hydrothermal method: 0.03mol Ca(NO 3 ) 2 , 0.01mol Al(NO 3 ) 3 9H 2 O was dissolved in 50mL of water, and 5g of the magnetic biochar prepared in step (2) was added, mixed well and set aside; then, under stirring conditions, a mixture containing 0.01mol NaOH and 0.02mol NaOH was added to the above mixed solution 2 CO 3 20mL mixed aqueous solution, and hydrothermally reacted at 140°C for 4h, after the reaction was completed, filtered, washed, and dried...
Embodiment 2
[0055] In order to investigate the effect of different reaction times, weigh 200g of soil that has passed through a 2mm mesh sieve, and pour it into a 1L beaker. Add 400mL of deionized water at a water-to-soil ratio of 2:1. After standing still for 1 h, 6 g of the modified magnetic biochar prepared in Example 1 was added at 1% of the soil mass, stirred for 30 min, and two parallel experiments were set up. After standing for 12h, 24h, 36h and 48h respectively, the magnetic biochar with adsorbed Cd was reclaimed with a magnet, and the removal rate of total cadmium in the measurement and calculation soil was as follows: image 3 shown.
[0056] The effect of different dosages, weigh 3 parts of 200g soil that has passed through a 2mm mesh sieve, and pour it into a 1L beaker. Add 400mL of deionized water at a water-to-soil ratio of 2:1. After standing still for 1h, add 1g, 2g and 4g of modified magnetic biochar (prepared in Example 1) respectively in the beaker with 0.5%, 1% and...
Embodiment 3
[0058] The air-dried soil passed through a 2mm sieve was subjected to particle size classification, the content of Cd in different particle sizes was measured, and the distribution of Cd content in different particle sizes was calculated. Clay particle size <0.002mm, powder particle size 0.002-0.02mm, sand particle size 0.02-2mm.
[0059] like Figure 5 As shown, the content of Cd in clay, silt and sand is 1.83, 1.42, 0.69mg / kg respectively, and it can be seen that the Cd concentration in clay is the highest. Therefore, removing a small part of clay can make the total amount of soil Cd reach reduction effect.
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