Color material dispersion liquid, photosensitive colored resin composition, color filter, liquid crystal display equipment, and organic light emitting display equipment
一种彩色滤光片、树脂组合物的技术,应用在色材分散液、感光性着色树脂组合物、彩色滤光片、液晶显示设备、及有机发光显示设备领域,能够解决着色树脂层剥离等问题,达到亮度高、溶剂再溶解性优异、色材分散稳定性优异的效果
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[0576] Examples are shown below to specifically describe the present invention. The present invention is not limited by these descriptions.
[0577] The acid value of the block copolymer before salt formation and the acid value of the salt-type block copolymer formed from the compound represented by the above general formula (2) are obtained by a method based on the method described in JIS K 0070 have to.
[0578] The amine value of the block copolymer before salt formation and the amine value of the salt-type block copolymer formed from the compound represented by the above general formula (2) are determined by the method based on the method described in JIS K 7237 have to.
[0579] The glass transition temperature (Tg) of the block copolymer before and after salt formation was measured by differential scanning calorimetry (DSC) (manufactured by SII Nano Technology Co., Ltd., EXSTARDSC 7020) for determination.
[0580] The weight average molecular weight (Mw) of the block...
Embodiment I
[0596] Example I Series: First Aspect of the Invention
Synthetic example 1
[0597] (Synthesis Example 1: Production of Block Copolymer A-1)
[0598]250 parts by mass of THF and 0.6 parts by mass of lithium chloride were added to a 500 mL round-bottomed four-necked separable flask equipped with a cooling tube, a funnel for addition, an air inlet for nitrogen, a mechanical stirrer, and a digital thermometer, and nitrogen replacement was sufficiently performed. . After cooling the reaction flask to -60°C, 4.9 parts by mass of butyllithium (15% by mass hexane solution), 1.1 parts by mass of diisopropylamine, and 1.0 parts by mass of methyl isobutyrate were injected using a syringe. 0.37 parts by mass of 1-ethoxyethyl methacrylate (EEMA), 18.6 parts by mass of 2-ethylhexyl methacrylate (EHMA), n-butyl methacrylate as monomers for the B block (BMA) 15.4 mass parts, benzyl methacrylate (BzMA) 9.5 mass parts, and methyl methacrylate (MMA) 29.3 mass parts were dripped over 60 minutes using the addition funnel. After 30 minutes, 27.0 parts by mass of dimethyl...
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