A process for extracting Dendrobium officinale extract from Dendrobium officinale at low temperature by heat reflux

A technology of dendrobium sheathing and heat reflux, which is applied in the field of heat reflux and low temperature extraction of dendrobium sheathing extract, can solve the problems of waste of resources, cumbersome extraction methods, low extraction rate of dendrobium sheathing extract, and achieve simple steps and easy manipulation Effect

Active Publication Date: 2021-09-14
贵州天诚农业科技发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] However, the above patent applications and the extraction method of the Dendrobium sheath extract in the prior art are relatively cumbersome, and the extraction rate of the Dendrobium sheath extract is not high, resulting in waste of resources

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030]A process for extracting Dendrobium dendrobii extract at low temperature by heat reflux from Dendrobium dendrobii, comprising the following steps: adding Dendrobium dendrobii and a solvent into an extraction tank for vacuum steam extraction, using ultrasonic wave to assist the extraction, and then sending it into a raw film for heating The raw film is heated in the evaporator, and after being evaporated and concentrated by the evaporator, it is sent to the precipitation tank through the stainless steel pump, and the supernatant liquid is collected after precipitation in the precipitation tank. , the dilute ethanol obtains concentrated ethanol through the preparation tank, and the concentrated solution is pulverized after being vacuum-dried or spray-dried to obtain the Dendrobium syringae extract; specifically, the following steps are included:

[0031] (1) Low temperature vacuum steam extraction: first put the fresh stems or dried stems of Dendrobium officinale into a was...

Embodiment 2

[0037] A process for extracting Dendrobium dendrobii extract at low temperature by heat reflux from Dendrobium dendrobii, comprising the following steps: adding Dendrobium dendrobii and a solvent into an extraction tank for vacuum steam extraction, using ultrasonic wave to assist the extraction, and then sending it into a raw film for heating The raw film is heated in the evaporator, and after being evaporated and concentrated by the evaporator, it is sent to the precipitation tank through the stainless steel pump, and the supernatant liquid is collected after precipitation in the precipitation tank. , the dilute ethanol obtains concentrated ethanol through the preparation tank, and the concentrated solution is pulverized after being vacuum-dried or spray-dried to obtain the Dendrobium syringae extract; specifically, the following steps are included:

[0038] (1) Low temperature vacuum steam extraction: first put the fresh stems or dried stems of Dendrobium officinale into a wa...

Embodiment 3

[0044] A process for extracting Dendrobium dendrobii extract at low temperature by heat reflux from Dendrobium dendrobii, comprising the following steps: adding Dendrobium dendrobii and a solvent into an extraction tank for vacuum steam extraction, using ultrasonic wave to assist the extraction, and then sending it into a raw film for heating The raw film is heated in the evaporator, and after being evaporated and concentrated by the evaporator, it is sent to the precipitation tank through the stainless steel pump, and the supernatant liquid is collected after precipitation in the precipitation tank. , the dilute ethanol obtains concentrated ethanol through the preparation tank, and the concentrated solution is pulverized after being vacuum-dried or spray-dried to obtain the Dendrobium syringae extract; specifically, the following steps are included:

[0045] (1) Low temperature vacuum steam extraction: first put the fresh stems or dried stems of Dendrobium officinale into a wa...

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PUM

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Abstract

The invention discloses a process for extracting an extract of Dendrobium sheathes from Dendrobium sheathes at low temperature under heat reflux, which comprises the following steps: adding Dendrobium sheathes and a solvent into an extraction tank for vacuum steam extraction, and ultrasonically assisted extraction, and then sending Enter the film heater to heat the film, after being evaporated and concentrated by the evaporator, it is sent to the sedimentation tank through a stainless steel delivery pump, and the supernatant is taken after precipitation in the sedimentation tank, and the supernatant is concentrated by a multifunctional alcohol recovery concentrator to obtain concentration liquid and dilute ethanol, dilute ethanol is obtained concentrated ethanol through a preparation tank, and the concentrated solution is vacuum-dried or spray-dried and then pulverized to obtain the Dendrobium sheath extract. The extraction method of the present application has simple steps and is easy to operate. After extraction by this method, the transfer rate of effective components of Dendrobium sheathes and the yield of Dendrobium dendrobii extracts are relatively high. 88.6%.

Description

technical field [0001] The invention belongs to the technical field of plant extraction processes, and in particular relates to a process for extracting Dendrobium officinale extracts from Dendrobium officinale at low temperature by heat reflux. Background technique [0002] Dendrobium is a famous yin-tonifying Chinese medicine, which has the functions of nourishing yin and clearing heat, promoting body fluid and benefiting the stomach, moistening the lungs and relieving cough, benefiting the kidneys and improving eyesight. Modern research has shown that it has the functions of anti-tumor, enhancing immunity, anti-platelet aggregation, improving vision, dilating blood vessels, and anti-oxidation. The genus Dendrobium is one of the largest genera of the orchid family, with more than 1,500 species in the world, widely distributed in tropical and subtropical regions such as Asia, Europe and Oceania. There are about 76 species in my country, mainly distributed in Southwest, Eas...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K36/8984
CPCA61K36/8984A61K2236/15A61K2236/17A61K2236/331A61K2236/51
Inventor 周高飞吴文伟
Owner 贵州天诚农业科技发展有限公司
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