Subcritical fluid continuous constant-pressure extraction and separation device system, and extraction and separation technology thereof

A subcritical fluid and extraction technology, applied in solid solvent extraction, separation methods, solvent extraction, etc.

Active Publication Date: 2019-08-23
SHANDONG UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0008] The purpose of the present invention is to overcome the defects existing in the existing subcritical fluid extraction dev...

Method used

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  • Subcritical fluid continuous constant-pressure extraction and separation device system, and extraction and separation technology thereof
  • Subcritical fluid continuous constant-pressure extraction and separation device system, and extraction and separation technology thereof
  • Subcritical fluid continuous constant-pressure extraction and separation device system, and extraction and separation technology thereof

Examples

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Embodiment 1

[0070] Embodiment 1: A subcritical fluid multi-stage continuous isobaric extraction and separation device system and process flow, such as figure 1 , figure 2 , Figure 6 , Figure 7 , Figure 11 shown.

[0071] A subcritical fluid multi-stage continuous isobaric extraction and separation device system consists of subcritical fluid medium source 5, pressurization subsystem 4, continuous extraction subsystem 1, first-stage separation subsystem 3-1,...,N-1 Stage separation subsystem 3-(N-1), N-stage separation subsystem 3-N, 1-stage pressurized cycle subsystem 2-1, ..., N-1 stage pressurized cycle subsystem 2-(N-1) Consists of an N-stage pressurized circulation subsystem 2-N, N is the total number of stages of step-by-step pressurization or extraction in the system, and N is greater than 2. The step-by-step extraction and step-by-step pressurization of subcritical fluids in the system of this embodiment coincide.

[0072] The subcritical fluid medium source 5 is composed ...

Embodiment 2

[0106] Embodiment 2: A subcritical fluid single-stage continuous isobaric extraction and separation device system and process flow, such as figure 1 , figure 2 , Figure 4 , Figure 6 , Figure 7 , Figure 10 , Figure 11 shown.

[0107] A subcritical fluid single-stage continuous isobaric extraction and separation device system consists of a subcritical fluid medium source 5, a pressurized subsystem 4, a continuous extraction subsystem 1, and a first-stage separation subsystem 3-1, ..., N-1 fractions Ion system 3-(N-1), N-level separation subsystem 3-N and 1-level pressurized circulation subsystem 2-1, ..., N-1-level pressurized circulation subsystem 2-(N-1), N The stage pressurization circulation subsystem is composed of 2-N, N is the total number of stages of step-up pressurization or extraction in the system, N is greater than 2, the subcritical fluid extraction in the system of this embodiment and the Nth pressure stage of step-by-step pressurization coincide.

...

Embodiment 3

[0132] Embodiment 3: a subcritical fluid multi-stage continuous isobaric extraction and separation device system and process flow for supercritical fluid pre-extraction, such as figure 1 , figure 2 , image 3 , Figure 6 , Figure 7 , Figure 8 , Figure 9 , Figure 11 shown.

[0133] A subcritical fluid multi-stage continuous isobaric extraction and separation device system for supercritical fluid pre-extraction consists of subcritical fluid medium source 5, pressurization subsystem 4, continuous extraction subsystem 1, first-stage separation subsystem 3-1,... , N-1 stage separation subsystem 3-(N-1), N-stage separation subsystem 3-N and 1-stage pressurized cycle subsystem 2-1,..., N-1 stage pressurized cycle subsystem 2-( N-1), N-level pressurized circulation subsystem 2-N constitutes, N is the step-by-step pressurization or extraction total number of stages in the system, N is greater than 2, the supercritical fluid and the subcritical fluid in this embodiment syste...

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Abstract

The invention relates to the field of chemical separation and bioengineering mechanical devices, and especially relates to a subcritical fluid continuous constant-pressure extraction and separation device system, and an extraction and separation technology thereof. The device system comprises a subcritical fluid medium source, a pressurization subsystem, a continuous extraction subsystem, a separation subsystem having the same step-by-step extraction or extraction stage number with the continuous extraction subsystem, and a pressurized circulation subsystem. The extraction and separation technology enforced by applying the extraction and separation system is operated to make a subcritical fluid or supercritical fluid in a bunker enter the corresponding separation subsystem after the completion of extraction in order to separate, and a discharge valve is periodically opened to discharge the extract separated by the separation subsystem. The device system and the technology have the advantages of high automation degree and reliable running of a device, reasonable process flow, realization of subcritical fluid continuous constant-pressure extraction and separation, energy saving, zeroemission, excellent processability and excellent separation effect.

Description

[0001] 1. Technical field [0002] The invention relates to the fields of chemical separation and bioengineering machinery equipment, in particular to a subcritical fluid continuous isobaric extraction and separation device system and an extraction and separation process. [0003] 2. Technical Background [0004] Subcritical fluid extraction and separation technology is another green chemical technology following supercritical fluid extraction and separation technology, and is being widely used in the field of extraction and separation. However, most of the existing subcritical fluid extraction devices are intermittent devices with quick-opening and sealed structures, which have low production efficiency and high energy consumption; frequent opening of the extractor has low safety and reliability and causes a great loss of extraction fluid, which is a serious constraint. application of this new technology. [0005] The Patent Office of the State Intellectual Property Office of...

Claims

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Application Information

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IPC IPC(8): B01D11/02
CPCB01D11/0203B01D11/0284
Inventor 王威强李飞曲延鹏李爱菊李冠忠李守军
Owner SHANDONG UNIV
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