A kind of preparation method and application of smoke yellow sunflower extract
A technology of extract and ambrette, which is applied in the preparation and application field of ambrette extract for tobacco, can solve the problems of limited application, high cost, and insufficient utilization of aroma components, and achieve good application prospects, Obvious effect
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Embodiment 1
[0023] 1. Adopt the ambrette fruit cortex as the extraction raw material, take ethyl acetate as the extractant, the mass ratio of the extractant to the ambrette fruit cortex is 5, extract at 40°C for 5 hours, separate the feed liquid, and concentrate the separated feed liquid to Extract, freeze-dried to obtain solid powder.
[0024] 2. Use ambrette dry leaves as extraction raw material, use 75% ethanol solution as extractant, the mass ratio of extractant to ambrette dry leaves is 20, extract at 60°C for 1 hour, separate the feed liquid, and concentrate the separated feed liquid into an extract .
[0025] 3. Use ambrette seeds as extraction raw materials, saturated saline and ether as extractants, and extract by distillation extraction at the same time. The mass ratio of saturated saline to ambrette seeds is 15, and the mass ratio of ether to ambrette seeds is 2. Adjust the heating temperature Make the distillation rate of the aqueous phase and the organic phase equal, extract...
Embodiment 2
[0028] 1. Use the ambrette fruit cortex as the extraction raw material, use ethyl acetate as the extractant, the mass ratio of the extractant to the ambrette fruit cortex is 15, extract at 70°C for 1 hour, separate the feed liquid, and concentrate the separated feed liquid to Extract, freeze-dried to obtain solid powder.
[0029] 2. Use the dried leaves of ambrette as extraction raw material, use 50% ethanol solution as the extractant, the mass ratio of the extractant to the dry leaves of ambrette is 15, extract at 75°C for 3 hours, separate the feed liquid, and concentrate the separated feed liquid into an extract .
[0030] 3. Adopt ambrette seed as extraction raw material, saturated saline and pentane are extractant, extract by distillation extraction at the same time, the mass ratio of saturated saline and ambrette seed is 20, the mass ratio of pentane and ambrette seed is 5, adjust Heating temperature makes the distilling rate of the aqueous phase and the organic phase e...
Embodiment 3
[0033] 1. Adopt the ambrette fruit cortex as the extraction raw material, use ethyl acetate as the extractant, the mass ratio of the extractant to the ambrette fruit cortex is 12, extract at 55°C for 2 hours, separate the feed liquid, and concentrate the separated feed liquid to Extract, freeze-dried to obtain solid powder.
[0034] 2. Use ambrette dry leaves as extraction raw materials, use 60% ethanol solution as extractant, the mass ratio of extractant to ambrette dry leaves is 10, extract at 85°C for 2 hours, separate the feed liquid, and concentrate the separated feed liquid into an extract .
[0035] 3. Ambrette seeds are used as extraction raw materials, saturated saline and isopentane are used as extractants, and extraction is carried out by distillation extraction at the same time. The mass ratio of saturated saline to ambrette seeds is 18, and the mass ratio of isopentane to ambrette seeds is 3. , adjust the heating temperature to make the distilling speed of the aq...
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