Opposite solid particle jet distributor online coke cleaning device
A solid particle, opposed technology, which is applied in the direction of cleaning heat transfer devices, non-rotating equipment cleaning, lighting and heating equipment, etc., can solve the problems of deterioration of the operating conditions of the reaction system, reduction of catalyst reaction performance, and increase of reactor operating pressure. Achieve the effect of strengthening gas-solid mixing effect, stabilizing reaction performance and maintaining consumption level
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Embodiment 1
[0034] Using the on-line decoking device for recycling solid particles of the present invention, a spray distributor is installed in the upper head of the cooler. The spray distributor is composed of 4 opposed nozzles. The pressure drop of the reaction gas cooler is 4kPa at the beginning of the start-up. Gas nitrogen is the driving force. The spherical iron ball particles with an average diameter of 5mm are transported to the opposed solid particle spray distributor through the solid particle feeder. After the distributor is sprayed, the solid particles are distributed to the spraying speed of 90m / s. In each tube of the ammoxidation reaction gas cooler, the coking material in the tube is cleared. When the acrylonitrile unit runs continuously for 24 months, the pressure drop of the cooler is 4.2kPa, which stabilizes the resistance and The operating pressure of the reaction system and the acrylonitrile unit yield of the catalyst remain unchanged, maintaining the consumption level ...
Embodiment 2~9
[0035] Operate according to the conditions and steps of Example 1, but change the type of inert gas, the average diameter of solid particles, the type of solid particles, the shape of solid particles, the ejection speed of solid particles, the type of distributor, the number of installations, The type and quantity of gas-solid separators, the operating conditions such as the ratio of the opening diameter of the protective plate to the inner diameter of the tube, the specific process operating conditions and the pressure drop of the reaction gas cooler after the device is running, the change in the single collection of acrylonitrile of the catalyst, and the operation of the device See Table 1 and Table 2 for the results of period, cooler tube sheet and tube scouring and wear.
[0036] Table 1 Comparison of process conditions between comparative examples and examples
[0037]
[0038]
[0039] Table 2 Comparison of device operation results between comparative examples and examples
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