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Recovering method for ultra-fine-grain ilmenite in inclined plate thickener overflow

A technology of ultra-fine particles and recovery methods, applied in the field of mineral processing engineering, can solve problems such as unsatisfactory recovery of ilmenite, inability to realize efficient use of resources, loss of titanium resources, etc.

Active Publication Date: 2019-03-08
KUNMING UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Production practice shows that the existing "strong magnetic separation + flotation" combined process and reagent system in the Panxi area has a good recovery effect on +38μm ilmenite, while -38μm ilmenite The ore recovery effect is not ideal, and the efficient utilization of resources cannot be realized; at the same time, this part of -38μm ultra-fine-grained ilmenite entering the coarse-grained flotation system will also deteriorate the flotation index of the coarse-grained grade, and the fine-grained titanium The recovery of iron ore has become a recognized problem in the titanium beneficiation industry
Therefore, inclined plate thickeners are usually used in production to concentrate and classify the magnetic separation concentrate, the underflow of the thickener (coarse-grained ilmenite) is used for flotation, and the overflow of the thickener (containing ultrafine-grained ilmenite) ) directly discarded into the tailings, which caused a large loss of titanium resources

Method used

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  • Recovering method for ultra-fine-grain ilmenite in inclined plate thickener overflow

Examples

Experimental program
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Effect test

Embodiment 1

[0018] A method for recovering ultra-fine-grained ilmenite in the overflow of an inclined-plate thickener. The raw material to be selected is a fine-grained ilmenite in the overflow of an inclined-plate thickener in Panzhihua, Sichuan, and TiO 2 Grade 15%, -38μm particle size above 95%, such as figure 1 As shown, the specific method is as follows: Concentrate the overflow of the inclined plate thickener to a pulp with a mass percent concentration of solids of 10wt%, and then subject the pulp to high-gradient magnetic separation for three times, one coarse and two fine, and the high gradient magnetic separation used in high-gradient magnetic separation The magnetic gathering medium of the magnetic separator is a rod medium and the diameter of the medium is 1mm. The rough separation magnetic induction intensity is 0.5T, and the magnetic induction intensity of the two selections is 0.3T. The magnetic separation rough concentrate is obtained, and water is added to adjust the rough...

Embodiment 2

[0020] A method for recovering ultra-fine-grained ilmenite in the overflow of an inclined-plate thickener. The ore to be selected is fine-grained ilmenite in the overflow of an inclined-plate thickener in Yunnan, TiO 2 The grade is 10%, and the particle size of -38μm is more than 85%. The specific method is as follows: Concentrate the overflow of the inclined plate thickener to a pulp with a mass percentage of solids of 20wt%, and conduct three high-gradient magnetic separations on the pulp. , the magnetic gathering medium of the high gradient magnetic separator used in high gradient magnetic separation is rod medium and the diameter of the medium is 1.5mm, the magnetic induction intensity of rough selection is 0.6T, and the magnetic induction intensity of the two selections is 0.4T, and the magnetic separation roughness is obtained. Concentrate, add water to adjust the mass percentage concentration of the rough concentrate to 22wt% Flotation desulfurization, flotation desulfu...

Embodiment 3

[0022] A method for recovering ultra-fine-grained ilmenite in the overflow of an inclined-plate thickener. The ore to be selected is fine-grained ilmenite in the overflow of an inclined-plate thickener in Yunnan, TiO 2 The grade is 12%, and the particle size of -38μm is more than 90%. The specific method is as follows: Concentrate the overflow of the inclined plate thickener to a pulp with a solid mass percentage concentration of 15wt%, and conduct three high-gradient magnetic separations on the pulp. , the magnetic gathering medium of the high gradient magnetic separator used in high gradient magnetic separation is a rod medium and the diameter of the medium is 1.8mm. Concentrate, add water to adjust the mass percentage concentration of the rough concentrate to 25wt% to obtain sulfur concentrate by flotation desulfurization, flotation desulfurization is a conventional prior art, add sulfuric acid to the desulfurization tailings to control the pulp pH=6, stir for 4min, and the...

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Abstract

The invention discloses a recovering method for ultra-fine-grain ilmenite in an inclined plate thickener overflow. Re-concentration is carried out on the inclined plate thickener overflow; then high-gradient magnetic separation is carried out; magnetic separation rough concentrate is adjusted to a proper flotation concentration for flotation desulfurization; and then after sulfuric acid, a combined inhibitor, and a composite collecting agent are sequentially added, roughing is carried out once, roughing bubbles are subjected to selection for three times, ore pulp in a roughing groove is subjected to scavenging once, the ore is sequentially returned to the previous operations in the selection process, and the bubbles are sequentially returned to the previous operations in the scavenging process. The recovery rate in the flotation operation is greater than 45%, and the grade of the titanium concentrate is 44%-47%.

Description

technical field [0001] The invention relates to a method for recovering ultrafine ilmenite in the overflow of an inclined plate thickener, belonging to the field of mineral processing engineering. Background technique [0002] my country's Panxi region is rich in vanadium-titanium magnetite resources, with proven reserves of 9.3×10 9 t, the ore contains more than ten beneficial components such as iron, vanadium, titanium, cobalt, nickel, copper, gallium, etc., among which the reserves of titanium resources account for more than 90% of the reserves of titanium resources in my country, and the comprehensive utilization value is extremely high. The main industrial minerals in the ore are titanomagnetite and ilmenite, which are the main raw materials for extracting iron and titanium respectively. At present, the overall technological process of selecting iron first and then titanium has been formed, that is, using weak magnetic separation to obtain iron concentrate with an iron...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03B9/06
CPCB03B9/06Y02W30/52
Inventor 刘建文书明王瑜曾勇王涵张松
Owner KUNMING UNIV OF SCI & TECH
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