Environmentally-friendly energy-saving emission reduction gasoline additive and preparation method thereof
A gasoline additive, energy-saving and emission-reducing technology, applied in the field of gasoline additives, can solve the problems of gasoline stability and adverse effects of combustion calorific value, etc.
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[0037] The preparation method of 3-phenyl-1-(2-amino-3,4,5-trimethoxy-phenyl) propenone at least comprises the following steps:
[0038] 0.8 mol of acetophenone and 0.7 mol of 2'-amino-3',4',5'-trimethoxyacetophenone were added to 0.8 ml of methanol in which 0.7 mol of cinnamaldehyde was dissolved. Add 0.4 mL of 6 mol / L sodium hydroxide solution to it, stir for 40 min, and refrigerate overnight. Filter, wash with ice water and methanol until neutral, and the methanol needs to be refrigerated for more than 12 hours before use. Purified by recrystallization to obtain 3-phenyl-1-(2-amino-3,4,5-trimethoxy-phenyl)propenone.
[0039] 2’-Amino-3’,4’,5’-trimethoxyacetophenone, CAS: 42465-69-0, was purchased from Hangzhou Jieheng Chemical Co., Ltd.
[0040] Acetophenone, CAS: 98-86-2, was purchased from Sinopharm Chemical Reagent Co., Ltd.
[0041] Cinnamaldehyde, CAS: 104-55-2, was purchased from Sinopharm Chemical Reagent Co., Ltd.
[0042] 3-Phenyl-1-(2-amino-3,4,5-trimethoxy-ph...
Embodiment 1
[0076] Embodiment 1 provides an environment-friendly energy-saving and emission-reducing gasoline additive, which at least includes the following components in parts by weight: 4 parts of ethyl tert-butyl ether, 2 parts of dimethyl carbonate, 3-phenyl-1-( 1 part of 2-amino-3,4,5-trimethoxy-phenyl)propenone, 2 parts of 3,4,5-trihydroxybenzamide, 1-(4-hydroxyphenyl)-5-mercapto- 3 parts of tetrazole, 1 part of benzotriazole, 4 parts of ethyl acetate, 6 parts of nitrobenzene, 2 parts of triethanolamine, 11 parts of isopentyl glycol, and 14 parts of solvent.
[0077] The preparation method of 3-phenyl-1-(2-amino-3,4,5-trimethoxy-phenyl) propenone at least comprises the following steps:
[0078] 0.8 mol of acetophenone and 0.7 mol of 2'-amino-3',4',5'-trimethoxyacetophenone were added to 0.8 ml of methanol in which 0.7 mol of cinnamaldehyde was dissolved. Add 0.4 mL of 6 mol / L sodium hydroxide solution to it, stir for 40 min, and refrigerate overnight. Filter, wash with ice water ...
Embodiment 2
[0083] Embodiment 2 provides an environment-friendly energy-saving and emission-reducing gasoline additive, which at least includes the following components in parts by weight: 9 parts of ethyl tert-butyl ether, 5 parts of dimethyl carbonate, 3-phenyl-1-( 3 parts of 2-amino-3,4,5-trimethoxy-phenyl)propenone, 6 parts of 3,4,5-trihydroxybenzamide, 1-(4-hydroxyphenyl)-5-mercapto- 9 parts of tetrazole, 5 parts of benzotriazole, 8 parts of ethyl acetate, 13 parts of nitrobenzene, 15 parts of isopentyl glycol, 5 parts of triethanolamine, and 30 parts of solvent.
[0084] The preparation method of 3-phenyl-1-(2-amino-3,4,5-trimethoxy-phenyl)propenone is the same as that in Example 1.
[0085] Described solvent is ethanol.
[0086] The preparation method of the environment-friendly energy-saving and emission-reducing gasoline additive is the same as in Example 1.
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