Preparation method of modified-porous-carbon-fiber-loaded calcium chloride hygroscopic material
A technology of porous carbon fiber and hygroscopic material, which is applied in the direction of carbon fiber, fiber chemical characteristics, fiber treatment, etc. It can solve the problems of low adsorption performance, difficulty in recycling, poor interfacial bonding between materials, etc., and achieve high hygroscopic strength and low cost of use , the effect of fast carbonization speed
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[0021] A method for preparing a modified porous carbon fiber loaded calcium chloride hygroscopic material, comprising the following steps:
[0022] (1) Mix calcium chloride and sodium carboxymethylcellulose at a mass ratio of 5:1 and dissolve in water with 2.5 times the mass to obtain a mixed salt solution for later use;
[0023] (2) Put the spinning solution in the electrospinning apparatus, wrap the receiver with aluminum foil, and collect the as-spun fibers on the aluminum foil. The process parameters of the spinning process are positive pressure 15kV, negative pressure 1.5kV, and advance rate 0.04 mm / min, the receiving rate is 30r / min, the distance between the needle and the receiver is 15cm, and the ambient temperature is 30°C. After the spinning is completed, let it stand at room temperature for one day to obtain the as-spun fiber, and then place it in an oven to raise the temperature. Solidify at 160°C for 60 minutes, take it out and put it into a tube furnace, raise th...
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