A method for preparing monophenolic compounds by microwave depolymerization of lignin
A monophenolic compound, lignin technology, applied in the preparation of organic compounds, chemical instruments and methods, organic chemistry, etc., can solve the problems of low degradation efficiency, high cost input, product quality constraints, etc., to improve efficiency and conversion. The effect of improving the efficiency and collection efficiency
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Embodiment 1
[0034] Taking the alkali lignin raw material as an example to introduce the implementation process of the present invention is as follows:
[0035] Mix 10g of alkali lignin (particle diameter 0.2-0.5mm, water content 8%) with 5g nano-silicon carbide particles (particle diameter 0.1-0.45mm) and perform microwave depolymerization reaction. In the microwave depolymerization reaction, a mixture of 100mL / min nitrogen, 1mL / min hydrogen and 10mL / min methanol was continuously introduced to start the microwave depolymerization reaction. The microwave depolymerization reaction conditions were microwave frequency 2.45GHz, microwave power 600W, heating temperature 500°C, reaction time 8 minutes. The thermal cracking vapor generated by microwave depolymerization is cooled at a condensation temperature of 1°C to obtain a solvent-based thermal cracking liquid. The solvent-based pyrolysis liquid is subjected to vacuum distillation, the vacuum distillation temperature is 20°C, and the relativ...
Embodiment 2
[0037] Taking the pyrolysis lignin raw material as an example to introduce the implementation process of the present invention is as follows:
[0038] Mix 10 g of pyrolytic lignin (particle size 0.05-0.1 mm, moisture content 3%) and 10 g of α-silicon carbide particles (particle size 0.45-1.0 mm) uniformly, and carry out microwave depolymerization reaction. In the microwave depolymerization reaction, a mixture of 300mL / min nitrogen, 3mL / min hydrogen and 150mL / min acetaldehyde was continuously introduced to start the microwave depolymerization reaction. The microwave depolymerization reaction conditions were microwave frequency 2.45GHz, microwave power 1200W, heating The temperature was 650°C, and the reaction time was 5 minutes. The thermal cracking vapor generated by microwave depolymerization is cooled at a condensation temperature of 5° C. to obtain a solvent-based thermal cracking liquid. The solvent-based thermal cracking liquid is subjected to vacuum distillation, the va...
Embodiment 3
[0040] Taking the lignosulfonate raw material as an example to introduce the implementation process of the present invention is as follows:
[0041] Mix 10g of lignosulfonate (particle size: 0.1-0.3mm, moisture content: 5%) with 8g of β-silicon carbide particles (particle size: 0.45-0.6mm) and perform microwave depolymerization reaction. In the microwave depolymerization reaction, a mixture of 200mL / min nitrogen, 2mL / min hydrogen and 50mL / min methyl formate was continuously introduced to start the microwave depolymerization reaction. The microwave depolymerization reaction conditions were microwave frequency 2.45GHz, microwave power 1000W, The heating temperature was 550° C., and the reaction time was 6 minutes. The pyrolysis vapor generated by microwave depolymerization is cooled at a condensation temperature of 3°C to obtain a solvent-based pyrolysis liquid. The solvent-based pyrolysis liquid is subjected to vacuum distillation, the vacuum distillation temperature is 30°C, an...
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