A continuous salting-out drying device and its application method
A drying device and salting-out technology, applied in separation methods, drying solid materials, chemical instruments and methods, etc., can solve the problems of many supporting equipment, poor working environment, long process flow, etc., to improve the working environment, simplify equipment, The effect of simplifying the process flow
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Embodiment 1
[0034] Salting out and drying treatment of pyridine aqueous solution with potassium hydroxide: prepare potassium hydroxide particles in the solid feed bin 7, open the solid feeding valve 8, and fill the drying section 5 with potassium hydroxide B, which has a water content of 42%. Pyridine aqueous solution A is pumped in with the feed pump 1, and the liquid level rises slowly. When the liquid touches the solid particles at the lower end of the drying section 5, the solution begins to dissolve potassium hydroxide. At this time, the solid feeding valve 8 is opened to stabilize the drying section 5. After the potassium hydroxide dissolved in the solution reaches a certain concentration, the feed liquid is layered, and the discharge of the waste water discharge pump 9 is adjusted through the oil-water interface meter to control the oil-water two-phase interface in the middle of the interface control section 4, and the pyridine aqueous solution A passes through the inlet The materia...
Embodiment 2
[0036] Triethylamine acetate aqueous solution is salted out with sodium hydroxide, drying treatment: the operation in embodiment 1 is basically the same, solid particles and aqueous solution are changed into sodium hydroxide and triethylamine acetate aqueous solution, and In the salting-out section, there is a chemical reaction and heat is released. It is necessary to add a jacket to the lower part of the tower and pass cooling water to cool down; the others are the same. The triethylamine acetate aqueous solution with a water content of 60% is subjected to alkali analysis and drying to obtain triethylamine with a water content of less than 0.1%, with a yield of 97%.
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