Oil-in-water-in-oil emulsion and preparation method thereof
A water-in-oil emulsion and water-emulsion technology, applied in the field of skin care products, can solve the problems of unstable emulsion, destruction of physical and chemical structure, loss of beneficial characteristics of consumers, etc., and achieve the effect of stable performance and no greasy feeling.
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[0069] The present invention also provides a kind of preparation method of water-in-oil-in-water emulsion, comprising the following steps:
[0070] A) mixing the oil phase in the first preservative, the first emulsifier, the flavor modifier and the water-in-oil emulsion evenly to obtain a mixed oil phase;
[0071] heating and mixing the mixed oil phase and the water phase in the water-in-oil emulsion, and homogenizing to obtain the water-in-oil emulsion;
[0072] B) mixing deionized water, humectant, second emulsifier, stabilizer and carbomer resin, and homogenizing to obtain an aqueous phase;
[0073] C) Heat and mix the water-in-oil emulsion and the water phase, then add 1,3 dimethylol-5,5 dimethylhydantoin and 2-methyl-4-isothiazoline- 3-ketone, mixed and stirred to obtain a water-in-oil-in-water emulsion;
[0074] Step A) and step B) are not limited in order.
[0075] In the present invention, firstly, the first preservative, the first emulsifier, the flavor regulator a...
Embodiment 1
[0097] 1. See Table 1 for the formula of water-in-oil-in-water emulsion inner layer water-in-oil emulsion
[0098] Table 1 Water-in-oil-in-water emulsion inner layer water-in-oil emulsion formula
[0099]
[0100]
[0101] 2. Preparation process of water-in-oil-in-water emulsion inner layer water-in-oil emulsion
[0102] 1) Add 1,3 dimethylol-5,5 dimethylhydantoin and polyglycerol-3-diisostearate into reaction pot 1, stir and mix until 1,3 dimethylol- After the 5,5-dimethylhydantoin is completely melted, add hydrogenated polydecene, isooctyl palmitate, olive oil in sequence, add essence, and mix well to obtain an oil phase;
[0103] 2) Add glycerin and water into the water phase pot 1, stir and mix evenly to obtain the water phase;
[0104] 3) Heat the oil phase to 85°C, and slowly add the water phase into the oil phase while stirring;
[0105] 4) Stir at constant temperature for 10 minutes and homogenize to obtain a water-in-oil emulsion.
[0106] 3. See Table 2 for...
Embodiment 2
[0121] 1. See Table 4 for the formula of water-in-oil-in-water emulsion inner layer water-in-oil emulsion
[0122] Table 4 water-in-oil-in-water emulsion inner layer water-in-oil emulsion formula
[0123]
[0124]
[0125] 2. Preparation process of water-in-oil-in-water emulsion inner layer water-in-oil emulsion
[0126] 1) Add 1,3 dimethylol-5,5 dimethylhydantoin and polyglycerol-3-diisostearate into reaction pot 1, stir and mix until 1,3 dimethylol- After the 5,5-dimethylhydantoin is completely melted, add hydrogenated polydecene, isooctyl palmitate, olive oil in sequence, add essence, and mix well to obtain an oil phase;
[0127] 2) Add glycerin and water into the water phase pot 1, stir and mix evenly to obtain the water phase;
[0128] 3) Heat the oil phase to 85°C, and slowly add the water phase into the oil phase while stirring;
[0129] 4) Stir at constant temperature for 10 minutes and homogenize to obtain a water-in-oil emulsion.
[0130] 3. See Table 5 for...
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