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Preparation method of energetic material with controllable interface infiltration performance

A performance and interface technology, applied in the direction of aromatic nitration composition, nitration acyclic/alicyclic/heterocyclic amine explosive composition, nitroalkane composition, etc., can solve the problem of uncontrollable surface and interface wetting properties, and achieve Good complete wetting and coating, good controllability of wetting performance, and the effect of reducing production costs

Active Publication Date: 2017-03-22
INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The present invention aims to solve the problem that the surface and interface wettability of the existing energetic materials cannot be adjusted during use, and a variety of bonding agents need to be selected, and provides a method for preparing energetic materials with controllable interface wettability

Method used

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  • Preparation method of energetic material with controllable interface infiltration performance
  • Preparation method of energetic material with controllable interface infiltration performance
  • Preparation method of energetic material with controllable interface infiltration performance

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A preparation method of an energetic material with controllable interface wettability includes the following steps:

[0029] Step 1. Ultrasonic dispersion of HMX particles with a particle size of 180μm in ethanol and water to a concentration of 5mg / ml, ultrasonic cleaning for 10min;

[0030] Step 2: After suction filtering the solid particles cleaned in step 1, they are placed in an oven at 80°C for 6h;

[0031] Step 3. Prepare 40ml of a 10mM tris buffer aqueous solution with a pH value of 8.5. Disperse the solid particles obtained in step 2 into the buffer solution, and add 2mg / mL dopamine hydrochloride to the dispersion Stir for 12h;

[0032] Step 4. The dispersion liquid that was stirred in step 3 was subjected to suction filtration and cleaning, and dried in an oven at 50°C for 5 hours;

[0033] Step 5, the TiO with a particle size of 20nm 2 The particles were added to deionized water at a concentration of 5 mg / ml, the dispersion was ultrasonically dispersed for 10 minutes, ...

Embodiment 2

[0038] The difference between this embodiment and the first embodiment is:

[0039] The solid particles mentioned in step one are RDX of 100 μm. Others are the same as the first embodiment.

Embodiment 3

[0041] The difference between this embodiment and the first embodiment is:

[0042] The solid particles mentioned in step one are 500 μm spherical HMX. Others are the same as the first embodiment.

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Abstract

The invention discloses a preparation method of an energetic material with controllable interface infiltration performance. The preparation method includes the steps that firstly, an energetic material with hydrophilicity is prepared; secondly, an energetic material wrapping specific nanometer particles is prepared; thirdly, washing and drying are conducted; fourthly, soaking with an alkyl siloxane solution is conducted; and fifthly, washing and drying are conducted, so that the energetic material with the controllable interface infiltration performance is obtained. The preparation method has the beneficial effects that expensive equipment and severe experiment conditions do not need to be used, and the production cost is reduced; the characteristics of convenience and rapidness are achieved, and good infiltration performance controllability is achieved; the energetic material which is prepared through the preparation method and has the controllable surface and interface infiltration performance is used for the field of PBX, the infiltration performance can be changed at any time according to changes of a bonding system, and a good solid-liquid complete infiltrating and wrapping effect is achieved; and water-insoluble energetic materials such as HMX, RDX and TATB can be used as modification matrixes, and the wide application range is achieved.

Description

Technical field [0001] The invention relates to a preparation method of an energetic material, in particular to a preparation method of an energetic material with controllable interface wettability, and belongs to the technical field of material preparation. Background technique [0002] Pouring polymer bonded explosives (PBX) with high-energy explosives such as Oktogen (HMX) and RDX (RDX) as the main charge contains a variety of components with different surface properties, solid-liquid, solid -The bonding force of the solid-phase interface is a major problem that plagues designers. Due to the problem of surface and interface wettability, it is usually necessary to add additives such as bonding agent during the use of the main explosive to make the explosive and other components in the PBX have better wettability and compatibility, and it is easy to form a uniformly coated mixture Explosive system is also one of the effective ways to improve the mechanical properties of PBX mol...

Claims

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Application Information

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IPC IPC(8): C06B25/34C06B25/04C06B25/40
CPCC06B25/04C06B25/34C06B25/40
Inventor 肖春祝青谢虓李尚斌罗观
Owner INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS
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