A kind of high-aroma tobacco extract, preparation method and application thereof
A tobacco extract and aroma technology, applied in the direction of tobacco, application, treatment of tobacco, etc., can solve the problems of weak aroma and high content of high-boiling substances, and achieve the effects of strong tobacco aroma, strong original tobacco aroma and good hair permeability.
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Embodiment 1
[0043] The high-aroma tobacco extract provided by this application is prepared through the following steps:
[0044] (1) Take 1 kg of flue-cured tobacco raw material, put it in a tobacco processing machine, spray propylene glycol evenly according to the proportion of 10% of the mass of tobacco raw material, seal it and place it for 12 h to make it fully absorbed; then heat it to 80 °C and bake it for 1.5 h ;
[0045] (2) Grinding the material after the baking in step (1), adding the extract to carry out low-temperature extraction; after the extraction, separate the mixture to obtain the extract;
[0046] When separating and obtaining the extract, specifically use a 400-mesh filter cloth to filter out the extract;
[0047]95% ethanol is used for the extract; the mass ratio of solid to liquid during extraction is 1:10 (that is, in terms of mass ratio, tobacco raw material:extract = 1:10);
[0048] For the low-temperature extraction, the extraction temperature is -20°C, and the...
Embodiment 2
[0055] The preparation method of the high-aroma tobacco extract provided in this example is the same as in Example 1, and only some parameters are adjusted as follows:
[0056] In step (1), the amount of propylene glycol sprayed is 5% of the tobacco mass, and after being sealed and placed for 6 hours, it is heated to 120°C and baked for 0.5 hours;
[0057] In step (2), the ratio of solid to liquid is 1:10, the extraction temperature is 40 °C, the extraction time is 3 h, and the extraction is performed twice;
[0058] In step (3), the ultrafiltration membrane filtration parameter is: 10 kD;
[0059] In step (4), during molecular distillation, the pressure was set at 0.01 mbar, and the distillation temperature was 20 °C.
[0060] The e-cigarette liquid prepared by using the high-aroma tobacco extract in this example uses propylene glycol as a solvent, dilutes the high-aroma tobacco extract to a mass concentration of 5%, and can be used directly.
Embodiment 3
[0062] The preparation method of the high-aroma tobacco extract provided in this example is the same as in Example 1, and only some parameters are adjusted as follows:
[0063] In step (1), the amount of propylene glycol sprayed is 20% of the tobacco mass, and after being sealed for 8 hours, it is heated to 140°C and baked for 1 hour;
[0064] In step (2), the ratio of solid to liquid is 1:8, the extraction temperature is 20 °C, the extraction time is 6 h, and the extraction is performed twice;
[0065] In step (3), the ultrafiltration membrane filtration parameter is: 8 kD;
[0066] In step (4), during molecular distillation, the pressure is set to 0.05mbar, and the distillation temperature is 30°C.
[0067] The e-cigarette liquid prepared by using the high-aroma tobacco extract in this example uses propylene glycol as a solvent, dilutes the high-aroma tobacco extract to a mass concentration of 3%, and can be used directly.
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