Garden tree fixing device with insecticidal system and working method of garden tree fixing device
A technology for fixing devices and trees, which can be applied to devices for catching or killing insects, cultivation, animal husbandry, etc. It can solve problems such as reduced efficiency and service life of fixing devices, high labor intensity, and large labor demand, and achieves device structure design Reasonable and compact, wide application range, good elasticity and strength
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Embodiment 1
[0053] Manufacture the fixed locking sleeve 1 of the present invention according to the following steps, and count by weight fraction:
[0054] Step 1: Add 700 parts of ultrapure water with a conductivity of 0.6μS / cm into the reactor, start the stirrer in the reactor at a speed of 110rpm, start the heating pump, and raise the temperature in the reactor to 35°C; add in order 10 parts of 2-n-undecyl-1,3-dioxane-5,5-dicarboxylic acid disodium salt, 4,5-dihydro-1-(2-hydroxyethyl)-hydroxide 1-carboxymethyl-2-undecyl-1H-imidazolium disodium salt 15 parts, 3,9-bis(octadecyloxy(alkyl))-2,4,8,10-tetraoxa- 30 parts of 3,9-diphosphospiro[5,5]undecane were stirred until completely dissolved, the pH value was adjusted to 4.5, the speed of the agitator was adjusted to 115 rpm, the temperature was 70°C, and the esterification reaction was carried out for 13 hours;
[0055] Step 2: Take 105 parts of 7-oxabicyclo[4.1.0]heptane-3,4-dicarboxylate bis(2-ethylhexyl)ester, 2,2'-[[2,2-di (Chlorome...
Embodiment 2
[0060] Manufacture the fixed locking sleeve 1 of the present invention according to the following steps, and count by weight fraction:
[0061] Step 1: Add 1800 parts of ultrapure water with a conductivity of 1.30μS / cm into the reactor, start the stirrer in the reactor at a speed of 220rpm, start the heating pump, and raise the temperature in the reactor to 75°C; add in order 45 parts of 2-n-undecyl-1,3-dioxane-5,5-dicarboxylic acid disodium salt, 4,5-dihydro-1-(2-hydroxyethyl)-hydroxide 46 parts of 1-carboxymethyl-2-undecyl-1H-imidazolium disodium salt, 3,9-bis(octadecyloxy(alkyl))-2,4,8,10-tetraoxa- 75 parts of 3,9-diphosphospiro[5,5]undecane were stirred until completely dissolved, the pH value was adjusted to 9.0, the speed of the agitator was adjusted to 340rpm, the temperature was 160°C, and the esterification reaction was carried out for 26 hours;
[0062] Step 2: Take 215 parts of 7-oxabicyclo[4.1.0]heptane-3,4-dicarboxylate bis(2-ethylhexyl)ester, 2,2'-[[2,2-di (Chl...
Embodiment 3
[0067] Manufacture the fixed locking sleeve 1 of the present invention according to the following steps, and count by weight fraction:
[0068] Step 1: Add 1,000 parts of ultrapure water with a conductivity of 1.1μS / cm into the reactor, start the stirrer in the reactor at a speed of 180rpm, start the heating pump, and raise the temperature in the reactor to 55°C; add in sequence 2-n-undecyl-1,3-dioxane-5,5-dicarboxylic acid disodium salt 25 parts, hydroxide 4,5-dihydro-1-(2-hydroxyethyl)- 30 parts of 1-carboxymethyl-2-undecyl-1H-imidazolium disodium salt, 3,9-bis(octadecyloxy(alkyl)yl)-2,4,8,10-tetraoxa- Stir 50 parts of 3,9-diphosphospiro[5,5]undecane until it is completely dissolved, adjust the pH value to 7.0, adjust the speed of the agitator to 240rpm, and the temperature is 110°C, and the esterification reaction takes 18 hours;
[0069] Step 2: Take 150 parts of 7-oxabicyclo[4.1.0]heptane-3,4-dicarboxylate bis(2-ethylhexyl) ester, 2,2'-[[2,2-di (Chloromethyl)-1,3-propyl...
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