Method for synthesizing gold nano-rod/graphene oxide composite material with one-pot process
A technology of gold nanorods and composite materials, applied in the nano field, can solve the problems of cumbersome operation and long time consumption, and achieve the effect of simple operation, short time consumption, green and mild reaction conditions
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0015] (1) Weigh an appropriate amount of graphene oxide and grind it, mix the ground 1mg graphene oxide with 0.1g polystyrene sodium sulfonate polymer solution for ultrasonic reaction (500-1000W, 30min), and then centrifuge, Redisperse the supernatant in 0.1 mL of water;
[0016] (2) Take 5mL of cetyltrimethylammonium bromide solution (0.2M), 625μL of chloroauric acid solution (0.008M), 3.975mL of deionized water, step (1) polymer-modified graphene oxide Solution, 300uL silver nitrate (0.004M), 12uL concentrated hydrochloric acid, 75uL ascorbic acid (85.8mM), 7.5uL sodium borohydride solution (0.01M) mixed and shaken for 30 seconds, kept at 25°C for 12h;
[0017] (3) Centrifuge the product obtained in step (2) at high speed (14000rpm, 20min), and redisperse the centrifuged substrate in water to obtain the final product.
[0018] figure 1 , figure 2 with image 3 It is a transmission electron microscope photograph of the prepared gold nanorod / graphene composite material,...
Embodiment 2
[0020] (1) Weigh an appropriate amount of graphene oxide and grind it, mix the ground 0.1mg graphene oxide with 0.1g polystyrene sodium sulfonate polymer solution for ultrasonic reaction (500-1000W, 30min), and then centrifuge , redisperse the supernatant in 1 mL of water;
[0021] (2) Take 5mL of cetyltrimethylammonium bromide solution (0.2M), 625μL of chloroauric acid solution (0.008M), 3.975mL of deionized water, the graphene oxide solution product of step (1), 300uL Silver nitrate (0.004M), 12uL concentrated hydrochloric acid, 75uL ascorbic acid (85.8mM), 7.5uL sodium borohydride solution (0.01M) were mixed and shaken for 30 seconds, and kept at a constant temperature of 30°C for 12h;
[0022] (3) Centrifuge the product obtained in step (2) at high speed (14000rpm, 20min), and redisperse the centrifuged substrate in water to obtain the final product.
[0023] The result is similar to Example 1.
Embodiment 3
[0025] (1) Weigh an appropriate amount of graphene oxide and grind it, mix the ground 0.1mg graphene oxide with 0.1g polystyrene sodium sulfonate polymer solution for ultrasonic reaction (500-1000W, 30min), and then centrifuge , redisperse the supernatant in 1 mL of water;
[0026] (2) Take 5mL of cetyltrimethylammonium bromide solution (0.2M), 625μL of chloroauric acid solution (0.008M), 3.975mL of deionized water, the graphene oxide solution product of step (1), 300uL Silver nitrate (0.004M), 12uL concentrated hydrochloric acid, 75uL ascorbic acid (85.8mM), 7.5uL sodium borohydride solution (0.01M) were mixed and shaken for 30 seconds, and kept at 25°C for 4 hours;
[0027] (3) Centrifuge the product obtained in step (2) at high speed (14000rpm, 20min), and redisperse the centrifuged substrate in water to obtain the final product.
[0028] The result is similar to Example 1.
PUM
Property | Measurement | Unit |
---|---|---|
Size length | aaaaa | aaaaa |
Diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com