A kind of lubricating oil and preparation method thereof
A lubricating oil and base oil technology, applied in the field of lubricating oil, can solve the problems of waste of manpower, waste of resources, environment, pollution, etc., and achieve the effect of less main components, simple preparation method and strong operability
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[0021] A method for preparing lubricating oil, comprising mineral base oil, poly-α-olefin (PAO), neopentyl polyol mixed fatty acid ester, zinc dialkyldithiophosphate, rare earth oxide; specifically comprising the following steps:
[0022] Get the mineral type base oil that is 50-60% by weight and the poly-alpha-olefin (PAO) that is 15-40% by weight, stir at T1 ℃ 1 hour to obtain mixed base oil A;
[0023] 7% by weight of neopentyl polyol mixed fatty acid ester and 1% by weight of borated fatty acid ester are added to the mixed base oil A, at T 2 Stir at t 2 Hour, obtain base oil B;
[0024] In the mixed base oil B, add 2% zinc dialkyldithiophosphate by weight, at T 3 Reaction at ℃ 3 Hour, obtain base oil C;
[0025] Add x% rare earth oxide powder to the base oil C, and react at 50-60°C for t 4 hours to obtain the final product.
[0026] The T 1 , T 2 , T 3 , satisfy the following relationship: 30≤T 2 1 3 ≤80, the unit is ℃. In order to fully disperse the zinc dialk...
Embodiment 1
[0030] Take the mineral type base oil that is 50% by weight and the poly-alpha-olefin (PAO) that is 35% by weight, stir at 50 ℃ for 4 hours to obtain mixed base oil A;
[0031] 7% by weight of neopentyl polyol mixed fatty acid ester and 1% by weight of borated fatty acid ester were added to the mixed base oil A, and stirred at 40°C for 2 hours to obtain base oil B ;
[0032] Adding 2% by weight of zinc dialkyldithiophosphate to the mixed base oil B, and reacting at 70°C for 1 hour to obtain base oil C;
[0033] Add x% oxidized rare earth powder to the base oil C, and react at 50-60° C. for 1 hour to obtain a finished oil.
[0034] The rare earth content x has the following relationship with the coefficient of friction of lubricating oil:
[0035] μ=exp[0.6224(lnx) 2 +3.6502lnx+e]±0.01, 0.01≤x≤0.15
[0036] Wherein, μ is the target friction coefficient of the lubricating oil, and x is the weight percentage of the rare earth content in the lubricating oil. The target fricti...
Embodiment 2
[0040] Get the mineral type base oil that is 50% by weight and the poly-alpha-olefin (PAO) that is 35% by weight, stir at 55 ℃ for 3 hours to obtain mixed base oil A;
[0041] 7% by weight of neopentyl polyol mixed fatty acid ester and 1% by weight of borated fatty acid ester were added to the mixed base oil A, and stirred at 40°C for 2 hours to obtain base oil B ;
[0042] Adding 2% by weight of zinc dialkyldithiophosphate to the mixed base oil B, and reacting at 75° C. for 1 hour to obtain base oil C;
[0043] Add x% oxidized rare earth powder to the base oil C, and react at 50-60° C. for 2 hours to obtain a finished oil.
[0044] The rare earth content x has the following relationship with the coefficient of friction of lubricating oil:
[0045] μ=exp[0.6224(lnx) 2 +3.6502lnx+e]±0.01, 0.01≤x≤0.15
[0046] Wherein, μ is the target friction coefficient of the lubricating oil, and x is the weight percentage of the rare earth content in the lubricating oil.
[0047] In gen...
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