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Double-frequency multichannel synchronization detection method for electric domain imaging

A synchronous detection, multi-channel technology, used in measurement devices, instruments, scanning probe microscopy, etc., can solve the problem of high-resolution imaging of excitation signals, etc., to improve detection accuracy, resolution, and reliability. The effect of noise ratio

Inactive Publication Date: 2015-12-09
UNIV OF ELECTRONICS SCI & TECH OF CHINA
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  • Abstract
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  • Application Information

AI Technical Summary

Problems solved by technology

In particular, when DC bias is applied on the needle tip to induce polarization reversal to observe the electric domain movement, due to the effect of the depolarization field, the above scanning method will inevitably affect the accuracy and efficiency of electric domain imaging.
In addition, the amplitude and frequency of the AC voltage often need to be determined according to specific experimental conditions, because the vertical piezoelectric response signal and the horizontal piezoelectric response signal are not completely consistent in response to frequency, and the signal-to-noise ratio is optimal. Piezoelectric response signals need to be obtained at different frequencies, so it is difficult to achieve high-resolution imaging of out-of-plane and in-plane electrical domains at the same time by relying on the previous single-frequency excitation signal

Method used

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  • Double-frequency multichannel synchronization detection method for electric domain imaging

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Embodiment Construction

[0018] The present invention will be described in further detail below with reference to the accompanying drawings and embodiments.

[0019] In this embodiment, the atomic force microscope used to detect the sample is a commercial scanning probe microscope, and the PFM module is composed of two lock-in amplifiers, two frequency sources (function generators), and a program-controlled computer, wherein the lock-in amplifier is a dual-phase lock-in amplifier. The probes for scanning and imaging on the sample surface are μMasch series Pt-coated Si conductive tips. To detect bismuth ferrite (BiFeO 3 ) film sample as an example, combined with the test system structure of electric domain imaging synchronous detection, such as figure 1 As shown, the specific measurement steps are as follows:

[0020] 1. Bismuth ferrite (BiFeO) with a bottom electrode 3 ) The thin film sample is placed on the sample stage of the atomic force microscope, and the conductive probe is used to contact t...

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Abstract

The invention belongs to the technical field of ferroelectric or piezoelectric material electric domain testing, and relates to a double-frequency multichannel synchronization detection method for achieving electric domain imaging through an inverse piezoelectric effect. The method employs two phase locking amplifiers to achieve the real-time synchronous detection of out-plane and in-plane piezoelectric signals of a to-be-tested sample. Reference signals of the two phase locking amplifiers are provided by two independent frequency sources, and the frequency sources also provide AC signals which are the same as the reference signals, wherein the AC signals serve as excitation signals. The excitation signals provided by the two frequency sources are superposed through an adder and then serve as AC excitation signals located between a conductive probe and the to-be-tested sample. The method can detect the amplitude and phase signals of the out-plane and in-plane piezoelectric vibration of the to-be-tested sample through one-time scanning, achieves multichannel synchronous output in a real-time mode, and greatly improves the detection efficiency. Meanwhile, the method can improve the resolution of electric domain imaging, and effectively improves the detection accuracy.

Description

technical field [0001] The invention belongs to the technical field of electric domain testing of ferroelectric or piezoelectric materials, and in particular relates to dual-frequency and multi-channel synchronous detection of electric domain imaging by utilizing the inverse piezoelectric effect. Background technique [0002] Ferroelectric material is a kind of dielectric material with spontaneous polarization behavior, its essential characteristic is to have spontaneous polarization, spontaneous polarization has two or more possible orientations, and spontaneous polarization can be turned under the action of external electric field. When the temperature is lower than the Curie temperature, the ferroelectric has a spontaneous polarization, and when the temperature is higher than the Curie temperature, the spontaneous polarization disappears. The spontaneous polarization in ferroelectric crystals, ferroelectric thin films, and ceramic grains is not uniformly distributed throu...

Claims

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Application Information

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IPC IPC(8): G01Q60/24
Inventor 曾慧中雷瑶罗文博帅垚张万里
Owner UNIV OF ELECTRONICS SCI & TECH OF CHINA
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