Composite collecting agent for sulphide ore and preparing method thereof
A composite collector and sulfide ore technology, applied in solid separation, flotation, etc., can solve the problems of increasing the difficulty and controllability of dosing, complicated dosing, and high cost of dosing, and achieve excellent collection effect and good selectivity , The effect of improving recovery indicators
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Embodiment 1
[0032] Embodiment 1: a kind of composite collector of sulfide ore, prepare following components: diisopropyl monothiophosphate 100kg, isopropyl monothioformate 190 kg, diisobutyl dithiophosphoric acid Sodium 350kg, C12 alcohol 80kg, dibutyl dithiocarbamate propionitrile 130kg, water 150kg.
[0033] Preparation steps:
[0034] (1) Prepare raw materials: sodium diisopropyl dithiophosphate, sodium isopropyl dithioxanthate, sodium chloroacetate, 10% NaOH solution;
[0035] Mix 240 kg of sodium diisopropyl dithiophosphate and 450 kg of sodium isopropyl dithioxanthate aqueous solution into the reactor, stir and add 330 kg of 41% sodium chloroacetate solution, and react at 55°C-60°C;
[0036] (2) After the reaction is complete, add 50kg of 10% NaOH solution and then heat up to 109°C for hydrolysis reaction. After the reaction, cool down to room temperature to obtain the mixed ester of the upper layer and the by-product flotation agent of the lower layer, and separate the mixed ester...
Embodiment 2
[0040] A composite collector for sulfide ore, prepare the following components: diisoamyl monothiophosphate 100kg, isobutyl monothioformate 200 kg, diisobutyl sodium dithiophosphate 400kg, C12 Alcohol 80 kg, dibutyl dithiocarbamate propionitrile 120 kg, water 100 kg.
[0041] Preparation steps:
[0042] (1) Prepare raw materials: sodium diisoamyl dithiophosphate, sodium isobutyl dithioxanthate, sodium chloroacetate, 10% NaOH solution;
[0043] Mix 135 kg of sodium diisoamyl dithiophosphate and 500 kg of sodium isobutyl dithioxanthate aqueous solution into the reactor, stir and add 535 kg of 41% sodium chloroacetate solution, and react at 55°C-60°C;
[0044] (2) After the reaction is complete, add 50kg of 10% NaOH solution and then heat up to 109°C for hydrolysis reaction. After the reaction is complete, cool down to room temperature to obtain the mixed ester of the upper layer and the by-product flotation agent of the lower layer, and separate the mixed ester of the upper...
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