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Composite collecting agent for sulphide ore and preparing method thereof

A composite collector and sulfide ore technology, applied in solid separation, flotation, etc., can solve the problems of increasing the difficulty and controllability of dosing, complicated dosing, and high cost of dosing, and achieve excellent collection effect and good selectivity , The effect of improving recovery indicators

Active Publication Date: 2015-08-12
YANTAI HUMON CHEM AUX CO LTD
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the prior art, a single flotation collector is often used in the flotation of sulfide ores. With the change and complexity of the ore, the single drug is gradually replaced by the compound drug that adds multiple collectors at the same time. The purpose is to use the synergistic collection of minerals to achieve a better mineral recovery rate and the desired concentrate grade. Although the compound drug improves the collection and selectivity of minerals, it increases the difficulty and difficulty of dosing. Controllability, high cost of medicine, complicated medicine

Method used

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  • Composite collecting agent for sulphide ore and preparing method thereof
  • Composite collecting agent for sulphide ore and preparing method thereof
  • Composite collecting agent for sulphide ore and preparing method thereof

Examples

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Embodiment 1

[0032] Embodiment 1: a kind of composite collector of sulfide ore, prepare following components: diisopropyl monothiophosphate 100kg, isopropyl monothioformate 190 kg, diisobutyl dithiophosphoric acid Sodium 350kg, C12 alcohol 80kg, dibutyl dithiocarbamate propionitrile 130kg, water 150kg.

[0033] Preparation steps:

[0034] (1) Prepare raw materials: sodium diisopropyl dithiophosphate, sodium isopropyl dithioxanthate, sodium chloroacetate, 10% NaOH solution;

[0035] Mix 240 kg of sodium diisopropyl dithiophosphate and 450 kg of sodium isopropyl dithioxanthate aqueous solution into the reactor, stir and add 330 kg of 41% sodium chloroacetate solution, and react at 55°C-60°C;

[0036] (2) After the reaction is complete, add 50kg of 10% NaOH solution and then heat up to 109°C for hydrolysis reaction. After the reaction, cool down to room temperature to obtain the mixed ester of the upper layer and the by-product flotation agent of the lower layer, and separate the mixed ester...

Embodiment 2

[0040] A composite collector for sulfide ore, prepare the following components: diisoamyl monothiophosphate 100kg, isobutyl monothioformate 200 kg, diisobutyl sodium dithiophosphate 400kg, C12 Alcohol 80 kg, dibutyl dithiocarbamate propionitrile 120 kg, water 100 kg.

[0041] Preparation steps:

[0042] (1) Prepare raw materials: sodium diisoamyl dithiophosphate, sodium isobutyl dithioxanthate, sodium chloroacetate, 10% NaOH solution;

[0043] Mix 135 kg of sodium diisoamyl dithiophosphate and 500 kg of sodium isobutyl dithioxanthate aqueous solution into the reactor, stir and add 535 kg of 41% sodium chloroacetate solution, and react at 55°C-60°C;

[0044] (2) After the reaction is complete, add 50kg of 10% NaOH solution and then heat up to 109°C for hydrolysis reaction. After the reaction is complete, cool down to room temperature to obtain the mixed ester of the upper layer and the by-product flotation agent of the lower layer, and separate the mixed ester of the upper...

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Abstract

The invention provides a composite collecting agent for sulphide ore and a preparing method thereof. The composite collecting agent comprises 10-15% of dialkyl monothiophosphate, 15-30% of alkyl monothioformate, 15-40% of dialkyl dithiophosphate, 5-10% of cosolvent, 13-15% of dialkyl dithiocarbamate and 10-20% of water. The composite collecting agent has the advantages that in use, the usage amount is small, cost is low, and the agents are added conveniently; the recovery indexes of metallic copper, gold, silver and the like are improved well; the composite collecting agent has composite action, collecting performance and foaming characteristic in the flotation process, also has the good selectivity and a superior collecting function for useful metal in clay-contained minerals, and can comprehensively recycle the useful metal minerals from complex minerals.

Description

technical field [0001] The invention belongs to the technical field of chemical industry, and in particular relates to a composite collector for sulfide ore and a preparation method thereof. Background technique [0002] In the prior art, a single flotation collector is often used in the flotation of sulfide ores. With the change and complexity of the ore, the single drug is gradually replaced by the compound drug that adds multiple collectors at the same time. The purpose is to use the synergistic collection of minerals to achieve a better mineral recovery rate and the desired concentrate grade. Although the compound drug improves the collection and selectivity of minerals, it increases the difficulty and difficulty of dosing. Controllability, the cost of the medicament is relatively high, and the medication is complicated. Contents of the invention [0003] In order to solve the above problems, the present invention provides a composite collector for sulfide ore ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B03D1/014B03D1/016B03D101/02B03D103/02
Inventor 曲华东鲁新州李先恩徐晓刘鹏徐庆华
Owner YANTAI HUMON CHEM AUX CO LTD
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