Preparation method of wheat straw charcoal
A wheat straw and biochar technology, which is applied in the field of biochar preparation, can solve the problem of low utilization rate of wheat straw, and achieve the effects of improving utilization rate and added value, good ecological and social benefits, and broad application prospects.
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[0023] Embodiments of the present invention provide a method for preparing wheat straw biochar, comprising the following steps:
[0024] Wheat straw is pulverized, mixed with water, and then introduced into a hydrothermal reaction kettle for hydrothermal carbonization reaction. The ratio of the mass of the wheat straw to the volume of water is 1kg:5L~1kg:15L; the product of the hydrothermal carbonization reaction is cooled , separated by filtration, and dried to obtain wheat straw biochar.
[0025] In the above technical solution, the present invention realizes the comprehensive utilization of wheat straw, increases the added value, and can fix carbon and reduce emissions, and obtains a product that can be used for environmental pollution restoration, and has better economic and social benefits.
[0026] As a preferred solution, the present invention also includes a pretreatment step of the wheat straw: removing residual roots of the wheat straw, and removing surface soil and ...
Embodiment 1
[0035] Such as figure 1 As shown, wheat straw biochar was prepared according to the following steps:
[0036] Step 1. Recycling and pretreatment of wheat straw: after the wheat is harvested, the remaining wheat straw is recovered, and the soil and sundries on the surface of the wheat straw are removed;
[0037] Step 2, crushing of wheat straw: crushing the wheat straw to obtain small particles and small lumps of raw materials (less than 1 cm in length), storing them for later use;
[0038] Step 3. Hydrothermal carbonization of wheat straw: mix wheat straw with water, introduce into a hydrothermal kettle, ensure that the hydrothermal kettle is airtight, heat for hydrothermal carbonization reaction, and the hydrothermal reaction temperature is 160 o C, reaction time 14 h, wheat straw raw material and water-solid-liquid ratio 1kg:15L;
[0039] Step 4. Filtration and separation of solid and liquid phase products: After the hydrothermal carbonization process, stop heating, and co...
Embodiment 2
[0042] Step 1. Recycling and pretreatment of wheat straw: after the wheat is harvested, the remaining wheat straw is recovered, and the soil and sundries on the surface of the wheat straw are removed;
[0043] Step 2, crushing of wheat straw: crushing the wheat straw to obtain small particles and small lumps of raw materials (less than 1 cm in length), storing them for later use;
[0044] Step 3. Hydrothermal carbonization of wheat straw: mix wheat straw with water, import it into a hydrothermal kettle, ensure that the hydrothermal kettle is airtight, and heat for hydrothermal carbonization reaction. The hydrothermal reaction temperature is 200 o C, reaction time 10 h, wheat straw raw material and water-solid-liquid ratio 1kg:10L;
[0045]Step 4. Filtration and separation of solid and liquid phase products: After the hydrothermal carbonization process, stop heating, and cool the hydrothermal reactor to below 80 o After C, open a still to export reaction solution and solid pha...
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