Content detection method of alprostadil injection
A technology of dil injection and detection method, applied in the field of content detection of alprostadil injection, can solve problems such as the reduction of β-naphthol peak area, and achieves improved detection precision, improved sampling precision, reliable column Effects of post-derivatization methods
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[0035] A kind of content detection method of alprostadil injection, the steps are: prepare β-naphthol internal standard solution; Need testing solution and reference substance solution are prepared into the β-naphthol internal standard solution containing identical concentration, then, adopt Alprostadil is separated by column by high performance liquid chromatography, and the post-column derivatization method is used as the reaction liquid in 1mol / L KOH solution, and the temperature of the reaction pool is 60°C. Finally, alprostadil and β -Naphthol peak area, calculate alprostadil content with internal standard method.
[0036] The preparation method of β-naphthol internal standard solution is to take 25 mg of β-naphthol, accurately weigh it, put it in a 50ml measuring bottle, add absolute ethanol to dissolve and dilute to the scale, measure 5ml, put it in a 50ml measuring bottle, add methanol to dilute To the mark, shake well, as the first solution; take 5ml of the first solu...
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