A kind of aluminum passivator and preparation method thereof
A technology of passivating agent and solution, which is applied in the coating process of metal materials, etc., which can solve the problems of decreased corrosion resistance, decreased discoloration and binding ability of die-casting aluminum surface, and failure to meet the requirements of practical applications, etc.
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Embodiment 1
[0027] A preparation method of passivating agent, comprising the following steps:
[0028] S1: Add 5 parts of silica sol, which is used as membrane skeleton, to water. In this embodiment, the silica sol is obtained by hydrolysis of silane. Silane is added to water, and the silica sol is produced by hydrolysis of silane.
[0029] S2: Fluozirconic acid for catalysis is also added, and the amount of said fluozirconic acid added is 3 parts. The fluozirconic acid here is used to catalyze the hydrolysis reaction of silane, which can make it form a silica sol skeleton more quickly. Fluorozirconic acid here is only a preferred embodiment because of its excellent catalytic effect. Other chemicals capable of catalyzing the hydrolysis of silanes are also possible.
[0030] S3: adding 1-3 parts by mass of flexible edible acid to it and mixing it to adjust the pH value to 3. In this embodiment, the flexible edible acid is 1 part of citric acid and 2 parts of glacial acetic acid.
[00...
Embodiment 2
[0035] A preparation method of passivating agent, comprising the following steps:
[0036] S1: Add 8 parts of silica sol, which is used as membrane skeleton, to water. In this embodiment, the silica sol is obtained by hydrolysis of silane. Silane is added to water, and the silica sol is produced by hydrolysis of silane.
[0037] S2: Fluozirconic acid for catalysis is also added, and the amount of said fluozirconic acid added is 5 parts. The fluozirconic acid here is used to catalyze the hydrolysis reaction of silane, which can make it form a silica sol skeleton more quickly. Fluorozirconic acid here is only a preferred embodiment because of its excellent catalytic effect. Other chemicals capable of catalyzing the hydrolysis of silanes are also possible.
[0038] S3: adding 1-3 parts by mass of flexible edible acid to it and mixing it to adjust the pH value to 3. In this embodiment, the flexible edible acid is 2 parts of citric acid and 3 parts of glacial acetic acid.
[0...
Embodiment 3
[0043] A preparation method of passivating agent, comprising the following steps:
[0044] S1: Add the silica sol used as the membrane skeleton into the water, 6 parts of the silica sol. In this embodiment, the silica sol is obtained by hydrolysis of silane. Silane is added to water, and the silica sol is produced by hydrolysis of silane.
[0045] S2: Fluozirconic acid used for catalysis is also added, and the amount of said fluozirconic acid added is 4 parts. The fluozirconic acid here is used to catalyze the hydrolysis reaction of silane, which can make it form a silica sol skeleton more quickly. Fluorozirconic acid here is only a preferred embodiment because of its excellent catalytic effect. Other chemicals capable of catalyzing the hydrolysis of silanes are also possible.
[0046] S3: adding 1-3 parts by mass of flexible edible acid to it and mixing it to adjust the pH value to 3. In this embodiment, the flexible edible acid is 2 parts of citric acid and 1 part of gla...
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