Activated carbon fiber paper and preparation method thereof
A technology of activated carbon fiber and precipitated fiber, which is applied in the direction of synthetic cellulose/non-cellulose material pulp/paper, fiber raw material treatment, papermaking, etc. Insufficient strength and other problems, to achieve the effect of good paper-forming property, excellent adsorption performance and high strength
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Embodiment 1
[0022] Preparation of meta-aramid fibrids: using isophthaloyl dichloride (IPC) and meta-phenylenediamine (MPD) as polymerization monomers, synthesize meta-aramid solution in dimethylacetamide (DMAc) system. The synthesized meta-aramid fiber solution is used to prepare the meta-aramid filtrate fiber. Among them, the concentration of meta-aramid fiber solution is 3%, and the coagulation bath H 2 The O / DMAc mixing weight ratio was 70:30, and the rotor speed was 2000 r / min.
[0023] Fiber paper preparation: The weighed meta-aramid fibrids were thawed with a beater at a beating concentration of 3% for 25 min to obtain a fibrous slurry with a beating degree of 55°SR. The chopped viscose-based activated carbon fibers with a weighed length of 3 mm were disintegrated with a beater at a beating concentration of 2% for 15 min to obtain an activated carbon fiber slurry with a beating degree of 15°SR. According to the ratio of the meta-aramid fibrid fiber accounting for 30% (based on the...
Embodiment 2
[0025] Preparation of meta-aramid fibrids: using isophthaloyl dichloride (IPC) and meta-phenylenediamine (MPD) as polymerization monomers, synthesize meta-aramid solution in dimethylacetamide (DMAc) system. The synthesized meta-aramid fiber solution is used to prepare the meta-aramid filtrate fiber. Among them, the concentration of the meta-aramid fiber solution is 5%, and the coagulation bath H 2 The O / DMAc mixing weight ratio was 60:40, and the rotor speed was 2500 r / min.
[0026] Preparation of fiber paper: The weighed meta-aramid fibrids were thawed with a beater at a beating concentration of 1% for 10 min to obtain a fibrous slurry with a beating degree of 40°SR. The chopped viscose-based activated carbon fibers with a weighed length of 1 mm were disintegrated with a beater at a beating concentration of 5% for 20 min to obtain an activated carbon fiber slurry with a beating degree of 20°SR. According to the proportion of meta-aramid fibrids accounting for 10% (based on ...
Embodiment 3
[0028] Preparation of para-aramid fibrids: Using terephthaloyl chloride (IPC) and p-phenylenediamine (MPD) as polymerization monomers, a para-aramid solution was synthesized in dimethylacetamide (DMAc) system. The synthesized para-aramid solution is used to prepare the para-aramid precipitated fiber. Among them, the concentration of para-aramid fiber solution is 7%, and the coagulation bath H 2 The O / DMAc mixing weight ratio was 70:30, and the rotor speed was 3000 r / min.
[0029] Preparation of fiber paper: The weighed para-aramid fibrids were thawed with a beater at a beating concentration of 5% for 30 min to obtain a fibrous slurry with a beating degree of 70 °SR. The chopped viscose-based activated carbon fibers with a weighed length of 8 mm were disintegrated with a beater at a beating concentration of 1% for 10 min to obtain an activated carbon fiber slurry with a beating degree of 10 °SR. According to the ratio of the para-aramid fibrid fiber accounting for 50% (based ...
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