Low-temperature water-based waterproof agent and production technology thereof
A water-repellent and water-based technology, applied in textiles, papermaking, fiber treatment, etc., can solve the problems of easy fire in the workshop, high production cost, hard hand feeling, etc., to prolong life and maintenance time, reduce cost consumption, glass transition temperature low effect
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Embodiment 1
[0015] A low-temperature water-based waterproofing agent of the present embodiment comprises the following components in weight percent: perfluoroalkyl ethyl acrylate C6 (Quzhou Jiangtian Fluorine Chemical Co., Ltd.) 28%; methyl methacrylate (Shanghai Bojing Chemical Co., Ltd.) Company) 18%; Octamethylcyclotetrasiloxane (Zhejiang Chuanhua Co., Ltd.) 15%; Octadecyltrimethylamine Chloride 5% (Jintan Organic Chemical Factory); Acetic acid 15%; Agent V-50 2%; deionized water 17%.
[0016] A production process of a low-temperature water-based waterproofing agent of the present embodiment comprises the following steps: 1) adding perfluoroalkyl ethyl acrylate C6, 50% octadecyltrimethylamine chloride, formazan 2) Use imported EmusiFlex-C3 high-pressure homogenizer with a pressure of 200MPa, pass through a 50nm filter membrane, and control the temperature at 85°C to homogenize the mixed solution in step 1). 3) according to the above ratio, adopt the SR-6000D type constant temperature ...
Embodiment 2
[0019] A low-temperature water-based waterproofing agent of the present embodiment comprises the following components in percentage by weight: perfluoroalkyl ethyl acrylate C6 (Quzhou Jiangtian Fluorine Chemical Co., Ltd.) 10%; octadecyl methacrylate (Shanghai Bojing Chemical Co., Ltd.) Co., Ltd.) 2%; Vinyltrimethoxysilane (Zhejiang Chuanhua Co., Ltd.) 1%; Octadecyltrimethylamine Chloride 0.1% (Jintan Organic Chemical Factory); Acetic acid 2%; Initiator V-50 0.1%; deionized water 84.8%.
[0020] The production process of a kind of low-temperature water-based water-repellent agent of the present embodiment comprises the following steps: 1) according to the above-mentioned proportion, the octadecyl trimethylamine chloride, acrylic acid Resin and water are mixed to form a mixed solution; 2) The imported EmusiFlex-C3 high-pressure homogenizer is used with a pressure of 200MPa to pass through a 50nm filter membrane and the temperature is controlled at 85°C to homogenize the mixed s...
Embodiment 3
[0023] A low-temperature water-based waterproofing agent of the present embodiment comprises the following components in percentage by weight: perfluoroalkyl ethyl acrylate C6 (Quzhou Jiangtian Fluorine Chemical Co., Ltd.) 20%; methyl methacrylate (Shanghai Bojing Chemical Co., Ltd.) company) 15%; r-(methacryloyloxy)propyltrimethoxysilane (Zhejiang Chuanhua Co., Ltd.) 8%; octadecyltrimethylamine chloride 2% (Jintan City Organic Chemical Factory ;) Acetic acid 8%; Initiator V-50 2%; Deionized water 45%.
[0024]The production process of a kind of low-temperature water-based water-repellent agent of the present embodiment comprises the following steps: 1) according to the above-mentioned proportion, the octadecyl trimethylamine chloride, acrylic acid Resin and water are mixed to form a mixed solution; 2) The imported EmusiFlex-C3 high-pressure homogenizer is used with a pressure of 200MPa to pass through a 50nm filter membrane and the temperature is controlled at 85°C to homogen...
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