Black reactive dye composition
A technology of reactive dyes and compositions, applied in organic dyes, dyeing methods, textiles and papermaking, etc., can solve the problems of high cost, complicated production process, insufficient blackness, etc., achieve high dyeing rate, good water solubility, and solve The effect of head and tail chromatic aberration
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[0007] The present invention provides A kind of black reactive dye composition, it comprises the following steps: Step 1, C.1. Synthesis of reactive black 5: put 150g of ice-water mixture in a beaker, weigh 56.2g of 100% para-ester, put the para-ester in the ice-water mixture for beating for 1 hour, add 30 % hydrochloric acid 24ml, then add 100% sodium nitrite 13.8g aqueous solution at 5-10°C, maintain 5-10°C, react with the reaction solution to the slightly blue color of starch potassium iodide test paper for 2 hours, eliminate it with sulfamic acid and add Zhebai H acid 33.1g, control the temperature at 15-18°C for 4 hours, adjust the pH value to 5-5.5 with baking soda and react for 3 hours, add a certain amount of stabilizer, and directly spray dry to get KN-B black finished product, chemical formula for:
[0008] Step 2, synthesis of mixed orange components: put ice-water mixture in a beaker, weigh 28.1g of 100% para-ester and 36.1g of 100% sulfonated para-ester, beat f...
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