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A kind of equipment for preparing catalytic cracking catalyst

A catalytic cracking and catalyst technology, applied in catalytic cracking, catalyst activation/preparation, physical/chemical process catalysts, etc., can solve problems such as device blockage, harmful hazards, and difficulty in improving, and achieve high production efficiency, low labor intensity, The effect of stable product performance

Active Publication Date: 2016-01-20
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this method uses gas to carry the molecular sieve powder material and SiCl 4 The gas phase ultrastable reaction is carried out by means of gas contact reaction. In order to fluidize the molecular sieve, the amount of gas must be large enough. The carrier gas and SiCl 4 The weight ratio can reach 10-250, otherwise it is easy to cause the problem of device blockage, increasing the amount of gas makes it difficult to increase the reaction depth, and there is a contradiction between the solid material transportation and the improvement of the gas phase ultra-stable reaction depth. A certain degree of reaction requires a larger SiCl 4 The amount of input will inevitably cause the residual SiCl after the gas phase ultrastable reaction 4 The increase in the amount of exhaust gas not only aggravates the harm of environmental pollution, but also is not conducive to the effective absorption of exhaust gas.

Method used

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  • A kind of equipment for preparing catalytic cracking catalyst
  • A kind of equipment for preparing catalytic cracking catalyst
  • A kind of equipment for preparing catalytic cracking catalyst

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preparation example Construction

[0029] In the method for preparing a catalytic cracking catalyst provided by the present invention, the molecular sieve is continuously introduced into the gas-phase superstable reactor, and the molecular sieve is continuously moved from the molecular sieve inlet to the molecular sieve outlet without carrier gas transportation, and reacts with the gas-phase superstable The silicon tetrachloride gas in the container is contacted to carry out the ultra-stabilizing reaction. Simultaneously, silicon tetrachloride was continuously introduced into the reactor.

[0030] In the method for preparing catalytic cracking catalyst provided by the present invention, silicon tetrachloride can be introduced in the reactor with liquid phase and then vaporized in the reactor and reacted with molecular sieves, but in order to make the reaction uniform, it is preferable to introduce silicon tetrachloride into the reactor after vaporization in a gas-phase ultrastable reactor. The molecular sieve ...

Embodiment approach

[0047] According to the second specific implementation of the equipment for preparing catalytic cracking catalyst provided by the present invention, a kind of gas phase superstable reactor such as image 3 As shown, the gas phase ultra-stable reactor comprises: reactor plate 11, baffle plate 21, molecular sieve inlet 31, gas phase silicon tetrachloride inlet 41, molecular sieve outlet 51, inner casing 61 and gas outlet 71, and this reactor also A tube rotation drive mechanism (not shown) may be included. Silicon tetrachloride and molecular sieve are respectively introduced in the space between sleeve pipe 61 and gas phase superstable reactor tube wall through silicon tetrachloride inlet 14 and molecular sieve inlet 31, and contact reaction, and wherein lifting plate 11 can make the Molecular sieve flipping is beneficial to the mixing of molecular sieve and silicon tetrachloride. The baffle plate 21 can prevent molecular sieve from sliding down along the reactor tube wall, whic...

Embodiment 1

[0069] Made of industrial grade stainless steel with a thickness of 3mm NiCr18Ti figure 2 In the molecular sieve gas-phase silicon replenishment equipment shown (the part after the roasting furnace), the upper part of the gas-solid separator 7 is cylindrical with a diameter of 6 meters and a height of 14 meters, and the lower part is a cone with an opening, and the cone angle is 45° , and the opening is provided with a valve, the discharge port is located at a position 1 meter away from the top of the gas-solid separator, and the absorption tower 7 is filled with a concentration of 10 mol / liter of sodium hydroxide aqueous solution, between the absorption tower 7 and the gas-solid separator 6 The room is connected by a catheter, and the catheter is deep in the sodium hydroxide aqueous solution.

[0070] Reactor 5 is a tubular reactor, such as Figure 5 As shown, the total length of the pipe body is 80 meters, and the diameter of the pipe body is 0.8 meters. The pipe body of t...

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Abstract

The invention relates to a device for preparing a catalytic cracking catalyst, which comprises a NaY molecular sieve exchange apparatus, a furnace, a gas phase ultra-stable reactor, a gas-solid separator and a gelatinizing device. The gas phase ultra-stable reactor comprises a molecular sieve inlet, a molecular sieve outlet and a silicon tetrachloride inlet; the gas phase ultra-stable reactor is capable of moving the molecular sieve from the molecular sieve inlet of the gas phase ultra-stable reactor to the molecular sieve outlet of the gas phase ultra-stable reactor under the condition that carrying gas is not used for conveying, and the molecular sieve and gas-phase silicon tetrachloride are contacted for reacting in the gas phase ultra-stable reactor. The apparatus can be used for continuously preparing a high silicon molecular sieve, the technology flow is simplified, carrying gas of the fluidization molecular sieve is not required, and the consumption of silicon tetrachloride can be greatly reduced.

Description

technical field [0001] The present invention relates to a kind of equipment for preparing catalytic cracking catalyst, and more specifically relates to a kind of equipment and its application for producing molecular sieve by using gas-phase chemical method to extract aluminum and supplement silicon, and then use the obtained molecular sieve to prepare catalytic cracking catalyst. Background technique [0002] Molecular sieve is a widely used material in catalytic cracking catalyst, and it is also a very important component. The performance of molecular sieve directly affects the reaction performance of catalytic cracking catalyst. According to different needs, molecular sieves can be modified differently to meet the requirements of use. For example, molecular sieves with a high silicon-to-aluminum ratio are generally considered to be required for catalytic cracking catalysts. [0003] In terms of preparing molecular sieves with high silicon-aluminum ratio, there are mainly ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J29/08B01J37/08B01J37/00C10G11/05
Inventor 张蔚琳朱玉霞田辉平周灵萍张杰潇许明德
Owner CHINA PETROLEUM & CHEM CORP
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