A kind of equipment for preparing catalytic cracking catalyst
A catalytic cracking and catalyst technology, applied in catalytic cracking, catalyst activation/preparation, physical/chemical process catalysts, etc., can solve problems such as device blockage, harmful hazards, and difficulty in improving, and achieve high production efficiency, low labor intensity, The effect of stable product performance
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preparation example Construction
[0029] In the method for preparing a catalytic cracking catalyst provided by the present invention, the molecular sieve is continuously introduced into the gas-phase superstable reactor, and the molecular sieve is continuously moved from the molecular sieve inlet to the molecular sieve outlet without carrier gas transportation, and reacts with the gas-phase superstable The silicon tetrachloride gas in the container is contacted to carry out the ultra-stabilizing reaction. Simultaneously, silicon tetrachloride was continuously introduced into the reactor.
[0030] In the method for preparing catalytic cracking catalyst provided by the present invention, silicon tetrachloride can be introduced in the reactor with liquid phase and then vaporized in the reactor and reacted with molecular sieves, but in order to make the reaction uniform, it is preferable to introduce silicon tetrachloride into the reactor after vaporization in a gas-phase ultrastable reactor. The molecular sieve ...
Embodiment approach
[0047] According to the second specific implementation of the equipment for preparing catalytic cracking catalyst provided by the present invention, a kind of gas phase superstable reactor such as image 3 As shown, the gas phase ultra-stable reactor comprises: reactor plate 11, baffle plate 21, molecular sieve inlet 31, gas phase silicon tetrachloride inlet 41, molecular sieve outlet 51, inner casing 61 and gas outlet 71, and this reactor also A tube rotation drive mechanism (not shown) may be included. Silicon tetrachloride and molecular sieve are respectively introduced in the space between sleeve pipe 61 and gas phase superstable reactor tube wall through silicon tetrachloride inlet 14 and molecular sieve inlet 31, and contact reaction, and wherein lifting plate 11 can make the Molecular sieve flipping is beneficial to the mixing of molecular sieve and silicon tetrachloride. The baffle plate 21 can prevent molecular sieve from sliding down along the reactor tube wall, whic...
Embodiment 1
[0069] Made of industrial grade stainless steel with a thickness of 3mm NiCr18Ti figure 2 In the molecular sieve gas-phase silicon replenishment equipment shown (the part after the roasting furnace), the upper part of the gas-solid separator 7 is cylindrical with a diameter of 6 meters and a height of 14 meters, and the lower part is a cone with an opening, and the cone angle is 45° , and the opening is provided with a valve, the discharge port is located at a position 1 meter away from the top of the gas-solid separator, and the absorption tower 7 is filled with a concentration of 10 mol / liter of sodium hydroxide aqueous solution, between the absorption tower 7 and the gas-solid separator 6 The room is connected by a catheter, and the catheter is deep in the sodium hydroxide aqueous solution.
[0070] Reactor 5 is a tubular reactor, such as Figure 5 As shown, the total length of the pipe body is 80 meters, and the diameter of the pipe body is 0.8 meters. The pipe body of t...
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