Large-pore composite plugging system and preparation method thereof
A technology of large channels and systems, applied in the direction of drilling compositions, chemical instruments and methods, etc., can solve the problems of short thermal stability time, failure to achieve plugging effect, short plugging validity period, etc., and achieve dispersion stability good effect
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Embodiment 1
[0029] The large-pore composite plugging system described in this example includes 1 kg of amphoteric polyacrylamide solution with a concentration of 0.2 wt%, 1 kg of cationic polyacrylamide solution with a concentration of 0.2 wt%, and 0.03 kg of a particle size of 100 mesh Active Calcium Carbonate.
[0030] The preparation method of the large-pore composite plugging system described in this embodiment comprises the following steps:
[0031] (1) Slowly add a specific amount of amphoteric polyacrylamide into a specific amount of oil field injection water with a salinity of 3000mg / L, stir at a stirring speed of 680r / min for 30min, then reduce the stirring speed to 420r / min, and continue stirring After 2 hours, a homogeneously mixed amphoteric polyacrylamide solution was obtained.
[0032] (2) Add a specific amount of activated calcium carbonate with a specific particle size to the amphoteric polyacrylamide solution in the step (1), stir for 15 min at a stirring speed of 680 r / ...
Embodiment 2
[0036] The large pore composite plugging system described in this example includes 1.5kg of amphoteric polyacrylamide solution with a concentration of 0.3wt%, 1kg of dodecyltrimethylammonium chloride solution with a concentration of 1wt%, and 0.075kg The particle size is 120 mesh active calcium carbonate.
[0037] The preparation method of the large-pore composite plugging system described in this embodiment comprises the following steps:
[0038] (1) Slowly add a specific amount of amphoteric polyacrylamide into a specific amount of oil field injection water with a salinity of 5000mg / L, stir at a stirring speed of 680r / min for 30min, then reduce the stirring speed to 420r / min, and continue stirring After 2 hours, a homogeneously mixed amphoteric polyacrylamide solution was obtained.
[0039] (2) Add a specific amount of activated calcium carbonate with a specific particle size to the amphoteric polyacrylamide solution in the step (1), stir for 15 min at a stirring speed of 6...
Embodiment 3
[0043] The macropore composite plugging system described in this example includes 2 kg of amphoteric polyacrylamide solution with a concentration of 0.35 wt%, 1 kg of dodecyldimethylbenzyl ammonium chloride solution with a concentration of 2.5 wt%, and The particle size of 0.12kg is 150 mesh fly ash.
[0044] The preparation method of the large-pore composite plugging system described in this embodiment comprises the following steps:
[0045] (1) Slowly add a specific amount of amphoteric polyacrylamide into a specific amount of oil field injection water with a salinity of 10,000mg / L, stir at a stirring speed of 700r / min for 30min, then reduce the stirring speed to 400r / min, and continue stirring Obtained after 1.8h, mixed homogeneous amphoteric polyacrylamide solution;
[0046] (2) Add a specific amount of fly ash with a specific particle size to the amphoteric polyacrylamide solution in the step (1), stir for 15 min at a stirring speed of 700 r / min, and stir evenly to obtai...
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