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Rapid detection method of chemical components illegally added in Chinese patent medicine Xiaohuoluo pills

A technology of Xiaohuoluo pills and chemical substances, which is applied in the field of rapid detection of illegally added chemical substances in Chinese patent medicine Xiaohuoluo pills, can solve the problems of inability to achieve rapid screening, high maintenance costs, and expensive instruments, and achieves false "positive" results. "The effect of interference, low cost and easy operation

Inactive Publication Date: 2015-05-27
焦琦
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, because infrared spectrometers, HPLC-MS, and GC-MS instruments are expensive and must be operated by professional technicians, the maintenance costs are also extremely high, and rapid screening cannot be achieved to achieve the purpose of monitoring

Method used

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  • Rapid detection method of chemical components illegally added in Chinese patent medicine Xiaohuoluo pills
  • Rapid detection method of chemical components illegally added in Chinese patent medicine Xiaohuoluo pills
  • Rapid detection method of chemical components illegally added in Chinese patent medicine Xiaohuoluo pills

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Embodiment Construction

[0023] Detailed examples are given below.

[0024] The present invention adopts: instruments and reagents: Sartoris BP211D electronic balance; AUTO SCIENCEAS10200BT type ultrasonic cleaner; P / G2007 type constant temperature oven; thin layer plate: silica gel GF 254Thin layer plate (Germany MERCK batch number: HX929689 Specification: 20×20cm); reagents are analytically pure; Prednisone reference substance (batch number: 100199-201002), triamcinolone acetonide reference substance (batch number: 100055-201103), hydrocortisone acetate reference substance (batch number: 100013-200607), acetaminophen reference substance (batch number: 100018-200408), dexamethasone reference substance (batch number: 100129-201105), cortisone acetate reference substance (batch number: 100123-200303), triamcinolone acetonide acetate reference substance (batch number: 100125-201105), phenylbutazone reference substance Products (batch number: 100481-200601), the above reference substances are provided b...

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Abstract

The invention relates to a rapid detection method of chemical components illegally added in Chinese patent medicine Xiaohuoluo pills. The method comprises the following steps: firstly, preparing a reference solution and a sample solution; respectively suctioning the reference solution and the sample solution; dripping on the same silica gel thin layer plate; adding a developing agent for ascending development; taking out and drying in the air; placing below an ultraviolet lamp and observing thin-layer chromatogram; spraying sulfuric acid-ethanol solution; placing in an oven and heating at a constant temperature until spots on the thin layer plate are clear; respectively placing below a fluorescent lamp and the ultraviolet lamp and observing thin-layer chromatogram; and determining that the sample result is positive if fluorescence quenching spots, fluorescence spots or spots with the same color occur at the same time at a point with a retardation factor value same as that of the reference. Obviously, the method provided by the invention is simple to operate, rapid, and cost-effective, not only solves the problem of false positive interference, but also avoids expensive cost and plenty of time consumed by the conventional infrared spectroscopy, HPLC-MS and the like, thereby making it possible to effectively monitor whether chemical components are illegally added in the Xiaohuoluo pills.

Description

technical field [0001] The invention relates to the field of quality detection of traditional Chinese medicines, in particular to a rapid detection method for illegally added chemical substances in Xiaohuoluo Pills, a Chinese patent medicine. Background technique [0002] Xiaohuoluo Pills is a traditional Chinese medicine preparation composed of 6 Chinese medicine decoction pieces including Dannanxing, Zhichuanwu, Zhicaowu, Dilong, frankincense (made) and myrrh (made). The main effects are dispelling wind and cold, resolving phlegm and dehumidification, promoting blood circulation and relieving pain. It is used for arthralgia caused by wind-cold-damp pathogen blockage and phlegm-stasis blockage of collaterals. Symptoms include limb joint pain, or cold pain, or tingling pain, or pain that is worse at night, joint flexion and extension difficulties, numbness and spasm. Its preparation method is to grind Dannanxing, Zhichuanwu, Zhicaowu, Dilong, frankincense (made), and myrrh ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90
Inventor 焦琦吴爱英张春辉
Owner 焦琦
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