A kind of preparation method of water-absorbing anti-fog glass
An anti-fog glass, water absorption technology, applied in the field of automotive glass, can solve the problems of fogging, short service life of anti-fog products, not resistant to wiping, etc., and achieve good anti-fog performance, convenient application, anti-aging and anti-fog performance Effect
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Embodiment 1
[0027] This embodiment provides a method for preparing water-absorbent anti-fog glass, comprising the following steps:
[0028] Add 5.5ml of tetraethyl orthosilicate and 2ml of distilled water into 80ml of ethyl acetate, and ultrasonically disperse to obtain a mixed solution. Dissolve 4.5ml of 25wt% saturated ammonia solution in 20ml of ethyl acetate at a speed of 3ml / min Add it into the above mixed solution at a uniform speed, keep the reaction temperature at 23-30°C during the reaction process, and keep ultrasonic action during the reaction process, and the reaction time is 3 hours to obtain nano Silica sol with a particle content of about 2.47wt% and a particle size of 2-20nm.
[0029] Dissolve 2.5g of silica sol in 2.5g of ethyl acetate, add non-ionic surfactant polyoxyethylene alkylphenol ether 0.25g, polyethylene glycol 600 (PEG600) 50mg, polyethylene glycol 400 (PEG400) 1.5 g, after stirring evenly, add 1.7 g of acrylic polyol resin and stir for 30 minutes, then add 2...
Embodiment 2
[0034] This embodiment provides a preparation method for anti-fog glass, comprising the following steps:
[0035] Add 7.5ml of tetraethyl orthosilicate and 4ml of distilled water to 80ml of acetone and mix, ultrasonically disperse to obtain a mixed solution, dissolve 6.5ml of 25wt% saturated ammonia solution in 20ml of acetone, and add it to the above mixing solution at a constant speed of 3ml / min solution, keep the reaction temperature at 23-30°C during the reaction, and keep ultrasonic in the reaction process, and the reaction time is 3 hours to obtain nano Silica sol with a particle content of about 3.27wt% and a particle size of 2-20nm.
[0036] Dissolve 2.5g of silica sol in 2.5g of acetylacetone, add non-ionic surfactant polyoxypropylene glycerol ether 0.25g, polyethylene glycol 600 (PEG600) 50mg, polyethylene glycol 400 (PEG400) 1.5g After stirring evenly, add 1.7g of acrylic polyol resin and stir for 30min, then add 2.8g of curing agent N3300, stir evenly to obtain a...
Embodiment 3
[0041] This embodiment provides a method for preparing an anti-fog composition for glass, comprising the following steps:
[0042] Add 5.5ml of tetraethyl orthosilicate and 4ml of distilled water to 85ml of isobutyl acetate and mix, ultrasonically disperse to obtain a mixed solution, dissolve 4ml, 25wt% saturated ammonia solution in 23ml of isobutyl acetate, at a speed of 3ml / min Add it into the above mixed solution at a uniform speed, keep the reaction temperature at 23-30°C during the reaction, keep ultrasonic during the reaction, and the reaction time is 3 hours to obtain nano Silica sol with a content of about 2.08wt% and a particle size of 2-20nm.
[0043] Dissolve 2.5g of silica sol in 2.5g of isobutyl acetate, add non-ionic surfactant polyoxypropylene glycerol ether 0.25g, polyethylene glycol 600 (PEG600) 50mg, polyethylene glycol 400 (PEG400) 1.5g, stir evenly, add 1.7g of acrylic polyol resin and stir for 30min, add 2.8g of curing agent N3300, stir evenly to obtain ...
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