ABS hydrophobic and oleophobic material with surface loaded by TiO2/diatomite, and preparation method thereof
A technology of surface loading and diatomite, applied in chemical instruments and methods, chemical/physical processes, physical/chemical process catalysts, etc., to achieve the effect of not easy to accumulate water vapor, simple manufacturing process, and low price
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Embodiment 1
[0026] A. Preparation of TiO 2 / Diatomite composite photocatalytic material:
[0027] (1) According to the volume ratio of butyl titanate, absolute ethanol and glacial acetic acid as 25:50:5, add analytical pure butyl titanate to analytical pure absolute ethanol, then add analytical pure glacial acetic acid, and then stir 30min to form a light yellow transparent solution A;
[0028] (2) According to the volume ratio of deionized water, analytically pure nitric acid and analytically pure absolute ethanol as 10:2:50, take deionized water and nitric acid and add them to absolute ethanol to obtain a transparent solution B;
[0029] (3) Stir diatomaceous earth and deionized water at a solid-to-liquid ratio (g / mL) of 8:100 to form a suspension, then add 1 mL of ferric nitrate solution with a concentration of 3 mol / L to the suspension, mix and stir evenly , so that the mass concentration of metal ions is 1%, and then adding a sodium hydroxide ethanol solution with a concentration o...
Embodiment 2
[0035] A. Preparation of TiO 2 / Diatomite composite photocatalytic material:
[0036] (1) According to the volume ratio of butyl titanate, absolute ethanol and glacial acetic acid as 20:48:2, add analytical pure butyl titanate to analytical pure absolute ethanol, then add analytical pure glacial acetic acid, and then stir 20min to form a light yellow transparent solution A;
[0037] (2) According to the volume ratio of deionized water, analytically pure nitric acid and analytically pure absolute ethanol as 13:3.5:47, take deionized water and nitric acid and add them to absolute ethanol to prepare a transparent solution B;
[0038] (3) Stir diatomite and deionized water at a solid-to-liquid ratio (g / mL) of 1:100 to form a suspension, then add lanthanum nitrate solution with a concentration of 1mol / L to the suspension, mix and stir evenly, Make the mass concentration of metal ions 0-5%, and then add a sodium hydroxide ethanol solution with a concentration of 3mol / L to it until...
Embodiment 3
[0044] A. Preparation of TiO 2 / Diatomite composite photocatalytic material:
[0045] (1) According to the volume ratio of butyl titanate, absolute ethanol and glacial acetic acid as 28:54:8, add analytical pure butyl titanate to analytical pure absolute ethanol, then add analytical pure glacial acetic acid, and then stir 50min to form a light yellow transparent solution A;
[0046] (2) According to the volume ratio of deionized water, analytically pure nitric acid and analytically pure absolute ethanol as 8:1:55, take deionized water and nitric acid and add them to absolute ethanol to obtain a transparent solution B;
[0047] (3) Stir diatomite and deionized water at a solid-to-liquid ratio (g / mL) of 12:100 to form a suspension, then add metal aluminum nitrate solution with a concentration of 6mol / L to the suspension, mix and stir evenly , so that the mass concentration of metal ions is 0 to 5%, and then adding a sodium hydroxide ethanol solution with a concentration of 5 m...
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