Rosemary extract and application thereof in cigarettes
A rosemary extract and rosemary technology, applied in the fields of application, tobacco, food science, etc., can solve problems that have not been reported, and achieve the effect of improving comfort, increasing economic value, and enriching the aroma of cigarettes
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Embodiment 1
[0022] Embodiment 1——Preparation and Application 1 of Rosemary Extract
[0023] 1. Preparation of Extracts
[0024] (1) Put the rosemary raw material into the extraction kettle, add 10% carrier agent (95% ethanol), and the supercritical CO 2 Inject into the extraction kettle, and extract for 3 hours under the conditions of extraction pressure of 20 MPa and extraction temperature of 30 °C, CO dissolved in aroma components 2 The fluid enters the separation tank, and the aroma components of rosemary are separated by reducing the pressure and increasing the temperature;
[0025] (2) Supercritical CO 2 The extracted material was molecularly distilled, and the light components separated under the conditions of feed rate of 60 g / h, scraping film speed of 500 r / min, distillation temperature of 40 °C and distillation pressure of 250 Pa were used as volatile oil .
[0026] (3) After diluting the volatile oil 50 times, the extract for perfuming is obtained.
[0027] 2. Cigarette Fla...
Embodiment 2
[0033] Embodiment 2——Preparation and Application 2 of Rosemary Extract
[0034] 1. Preparation of Extracts
[0035] (1) Put the rosemary raw material into the extraction kettle, add 10% carrier agent (95% ethanol), and the supercritical CO 2 Inject into the extraction kettle, and extract for 1 h under the conditions of extraction pressure of 40 MPa and extraction temperature of 50 °C, CO dissolved in aroma components 2 The fluid enters the separation tank, and the aroma components of rosemary are separated by reducing the pressure and increasing the temperature;
[0036] (2) Supercritical CO 2 The extracted material was molecularly distilled, and the light component obtained by separation under the conditions of feed rate of 85 g / h, scraping film speed of 600 r / min, distillation temperature of 60 °C and distillation pressure of 350 Pa was used as the volatile oil .
[0037] (3) After diluting the volatile oil 50 times, the extract for perfuming is obtained.
[0038] 2. Ci...
Embodiment 3
[0044] Embodiment 3——Preparation and Application 3 of Rosemary Extract
[0045] 1. Preparation of Extracts
[0046] (1) Put the rosemary raw material into the extraction kettle, add 10% carrier agent (95% ethanol), and the supercritical CO 2 Inject into the extraction kettle, and extract for 2 hours under the conditions of extraction pressure of 30 MPa and extraction temperature of 40 °C, CO dissolved in aroma components 2 The fluid enters the separation tank, and the aroma components of rosemary are separated by reducing the pressure and increasing the temperature;
[0047] (2) Supercritical CO 2 The extracted material was molecularly distilled, and the light component obtained by separation under the conditions of feed rate of 70 g / h, scraping film speed of 550 r / min, distillation temperature of 50 °C and distillation pressure of 300 Pa was used as volatile oil .
[0048](3) After diluting the volatile oil 50 times, the extract for perfuming is obtained.
[0049] 2. Cig...
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