Polymer for increasing speed for spinning fine-denier filaments in Nisshinbo dry process
A technology of fine denier silk and polymer, which is applied in the manufacture of rayon, textiles and papermaking, mono-component polyamide rayon, etc. The effect of increasing production capacity, increasing concentration and reducing cost
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Embodiment 1
[0021] The polytetramethylene ether glycol in the tank car is transported to the storage tank through a gear pump, and then measured by a mass flow meter, and about 867kg of polytetramethylene ether glycol is transported to the pre-polymerization reactor, and in addition The metering tank measures 4,4'-diphenylmethane diisocyanate, measures 201kg, and sends it to the pre-polymerization reactor, and reacts under the condition of 65°C heat preservation water. After about 100 minutes, the pre-polymerization ends, and the pre-polymerization transferred to the polymerization reactor.
[0022] In the polymerization reactor, the pre-polymer is cooled to about 10°C, and then ethylenediamine 17.34kg, propylenediamine 4.36kg and di-n-butylamine 5.27kg are added dropwise, according to the power curve of the polymerization reactor stirrer to determine the end point of the polymerization reaction. After the reaction was finished, 9.76kg of anti-yellowing agent, 4.80kg of antioxidant and 4...
Embodiment 2
[0024] The polytetramethylene ether glycol in the tank car is transported to the storage tank through a gear pump, and then measured by a mass flow meter, and about 860kg of polytetramethylene ether glycol is transported to the pre-polymerization reactor, and in addition The metering tank measures 4,4'-diphenylmethane diisocyanate, measures 201kg, and sends it to the pre-polymerization reactor, and reacts under the condition of 65°C heat preservation water. After about 100 minutes, the pre-polymerization ends, and the pre-polymerization transferred to the polymerization reactor.
[0025] The prepolymer is cooled to about 10°C in the polymerization reactor, and then ethylenediamine 17.76kg, propylenediamine 4.47kg and di-n-butylamine 4.93kg are added dropwise, according to the power curve of the polymerization reactor stirrer to determine the end point of the polymerization reaction. After the reaction, 9.61kg of anti-yellowing agent, 4.73kg of antioxidant and 4.73kg of light ...
Embodiment 3
[0027] The polytetramethylene ether glycol in the tank car is transported to the storage tank through a gear pump, and then measured by a mass flow meter, and about 863kg of polytetramethylene ether glycol is transported to the pre-polymerization reactor, and in addition The metering tank measures 4,4'-diphenylmethane diisocyanate, measures 201kg, and sends it to the pre-polymerization reactor, and reacts under the condition of 65°C heat preservation water. After about 100 minutes, the pre-polymerization ends, and the pre-polymerization transferred to the polymerization reactor.
[0028] In the polymerization reactor, the pre-polymer is cooled to about 10°C, and then ethylenediamine 17.66kg, propylenediamine 4.44kg and di-n-butylamine 4.70kg are added dropwise, according to the power curve of the polymerization reactor stirrer to determine the end point of the polymerization reaction. After the reaction was finished, 9.64kg of anti-yellowing agent, 4.75kg of antioxidant and 4...
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