Composite fiber and preparation method thereof
A composite fiber and cellulose technology, which is applied in fiber treatment, spinning solution preparation, cellulose/protein conjugated artificial filament, etc., can solve the problems of kapok fiber spinning difficulty, and achieve the solution of spinning difficulty and production cost Low, easy to produce effects
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Embodiment 1
[0038] The average particle size of the cleaned kapok fiber powder is 68.5 μm, soaked in 35% sodium hydroxide aqueous solution at a ratio of 1:2.5,
[0039] Mix the kapok fiber powder thoroughly and disperse in an ultrasonic oscillator for 4.5 hours at a temperature of 26°C. A kapok fiber powder solution is obtained.
[0040] In addition, the cellulose bamboo pulp with a polymerization degree of 550 is prepared by conventional cellulose viscose preparation processes such as alkali staining, pressing, crushing, aging, yellowing, dissolving, mixing, filtering, aging and degassing to obtain cellulose viscose spinning Stock solution, control the composition of this viscose spinning stock solution to be α cellulose 8.8%, contain alkali 4.5%.
[0041] Then get the kapok fiber powder solution and the cellulose spinning stock solution according to the production needs, mix and pass through no less than 10 minutes in a static mixer. 5 Mix for the first time to mix evenly. After pre-f...
Embodiment 2
[0043] Take the cleaned kapok fiber powder with an average particle size of 72.8 μm, soak it in 30% sodium hydroxide aqueous solution at a ratio of 1:3, fully mix the kapok fiber powder, and disperse it in an ultrasonic oscillator for 5 hours. is 25°C. A kapok fiber powder solution is obtained.
[0044] In addition, the cellulose hemp pulp with a degree of polymerization of 580 and the cellulose bamboo pulp with a degree of polymerization of 750 are processed by alkali staining, pressing, crushing, aging, yellowing, dissolving, mixing, filtering, aging and degassing. The cellulose viscose spinning stock solution is obtained in the viscose preparation process, and the composition of the viscose spinning stock solution is controlled to be 8.8% of α-cellulose and 4.5% of alkali.
[0045] Then get the kapok fiber powder solution and the cellulose spinning stock solution according to the production needs, mix and pass through no less than 10 minutes in a static mixer. 5 Mix for t...
Embodiment 3
[0047] Take the cleaned kapok fiber powder with an average particle size of 72.8 μm, soak it in 30% sodium hydroxide aqueous solution at a ratio of 1:3, fully mix the kapok fiber powder, and disperse it in an ultrasonic oscillator for 5 hours. is 25°C. A kapok fiber powder solution is obtained.
[0048] In addition, the cellulose bamboo pulp with a degree of polymerization of 780 and the cellulose straw pulp with a degree of polymerization of 450 are subjected to alkali staining, pressing, crushing, aging, yellowing, dissolving, mixing, filtering, ripening and degassing. The cellulose viscose spinning stock solution is obtained in the plain viscose preparation process, and the composition of the viscose spinning stock solution is controlled to be 8.8% of α-cellulose and 4.5% of alkali.
[0049] Then get the kapok fiber powder solution and the cellulose spinning stock solution according to the production needs, mix and pass through no less than 10 minutes in a static mixer. 5...
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