Olefin-based rubber highly flame-retardant and oil-resistant heat-shrinkable sleeve and preparation method thereof
A heat-shrinkable sleeve and high flame-retardant technology, which is applied to tubular objects, other household appliances, applications, etc., can solve the problems of high vulcanization cost, high vulcanization cost, and slow vulcanization speed, and achieve high flame-retardant performance and strong price Advantages, excellent oil resistance effect
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[0021] An olefin-based rubber highly flame-retardant and oil-resistant heat-shrinkable sleeve and a preparation method thereof, the preparation method sequentially comprising the following steps:
[0022] Step 1: Preparation of product pellets: Add 60-80Kg EPDM (EPDM rubber, imported from Japan, model EP57P), 20-10KgEEA, 20-10KgPOE, 5-10Kg methyl Vinyl silicone rubber, then start the internal mixer, the internal mixing temperature is 80-130 ℃, internal mixing 1-2 minutes; then add 100-120Kg magnesium hydroxide, 5-10Kg zinc borate, 0.5-1Kg methyl phenyl silicone oil, 0.3-0.6Kg antioxidant 1, 0.2-0.3Kg, antioxidant 2, 0.2-0.3Kg, cross-linking agent TMPTMA, 3-5Kg No. 10 white oil, 0.5-1Kg zinc stearate, 1-2Kg paraffin wax In the internal mixer, continue banburying for 7-8 minutes, and then discharge the banburyed materials into the parallel twin-screw granulation unit, melt and extrude, pelletize the underwater die surface, dry the particles after dehydration, and prepare Finish...
Embodiment 1
[0040] Embodiment 1: An olefinic rubber high flame-retardant and oil-resistant heat-shrinkable sleeve and its preparation method, the preparation method comprises the following steps in sequence:
[0041] Step 1: Preparation of product pellets: Add 60Kg EPDM (grafted modified EPDM rubber, grafted monomer: AN (acrylonitrile), grafting rate 15%) to the internal mixer in the following order, 20KgEEA (ethylene-octene copolymer, EA content 30%, ethyl acrylate content (weight), 20KgPOE (ethylene-octene copolymer, model POE8656), 5Kg methyl vinyl silicone rubber (type 110-2, molecular weight 650000, vinyl content 0.16%), then start the mixer, mixer temperature 80-130 ℃, mixer 1-2 minutes; then add 100 Kg magnesium hydroxide, 5Kg zinc borate, 0.5Kg methyl phenyl silicone oil, Add 0.2Kg antioxidant 1 (70% antioxidant 1010+30% antioxidant DSTDP), 0.2Kg antioxidant 2, 0.3Kg crosslinking agent TMPTMA, 3Kg white oil, 0.5Kg zinc stearate, 1Kg paraffin Put it into the internal mixer, contin...
Embodiment 2
[0046] With embodiment 1, the difference is the first step: get 80KgEPDM, 10KgEEA, 10KgPOE, 10Kg methyl vinyl silicone rubber, 120Kg magnesium hydroxide, 10Kg zinc borate, 1Kg methylphenyl silicone oil, 0.3Kg antioxidant 1 (antioxidant 300), 0.3Kg antioxidant 2, 0.6Kg crosslinking agent TMPTMA, 5Kg white oil, 1Kg zinc stearate, 2Kg paraffin.
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