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Polymer reactor for synthesizing rubber

A polymerization reactor and synthetic rubber technology, applied in chemical instruments and methods, chemical/physical processes, etc., can solve the problems of downtime, glue removal, cleaning, bonding condenser tube bundles, affecting production volume, etc., to save electricity and improve flow diversion. effect of speed

Inactive Publication Date: 2012-10-10
宋晓轩
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are multiple groups of condenser tube bundles arranged around the reactor, and the bottom of the reactor center is equipped with an axial-flow scraper heat dissipation stirring blade, which plays the role of mixing, stirring and heat dissipation. The length of the stirring shaft is straight from the bottom of the reactor center. At the top of the reaction kettle, the stirring power is as high as 315kw or more; and because the generated slurry moves upward in an irregular turbulent flow, the colloidal particles stick to the condensation tube bundle and block the slurry output pipe
Under normal operating conditions, work must be stopped every 2 months for glue removal and cleaning, which affects production

Method used

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  • Polymer reactor for synthesizing rubber
  • Polymer reactor for synthesizing rubber
  • Polymer reactor for synthesizing rubber

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] Embodiment 1, with reference to figure 1 , figure 2 , a vertical polymerization reactor for synthesizing butyl rubber, mainly comprising a reactor 1, multiple groups of condensation tube bundles 4 uniformly arranged around the inside of the reactor 1, and feed ports 9 uniformly distributed along the radial direction and height of the reactor 1 , the bottom center of the reactor 1 is equipped with a screw propeller 12, which can push the liquid flow upward; the screw propeller 12 is only at the bottom of the reactor 1, and the first motor 7 is connected to the outer end of the reactor 1 , the first motor 7 is an adjustable speed motor, and its power is only 55-110kw.

[0016] Catalyst feed pipe 10 and paddle type agitator 11 are all equipped with catalyst feed pipe 10 and paddle type agitator 11 on described reactor 1 radial direction and the uniform feed inlet 9 of height, can promote liquid lateral movement; The connecting shaft of this paddle type agitator 11 A sec...

Embodiment 2

[0019] Embodiment 2, with reference to image 3 , Figure 4 , a horizontal polymerization reactor for synthesizing butyl rubber, mainly comprising a reactor 1, which can be horizontally placed in the frame of the production device, and a plurality of groups of condensing tube bundles arranged uniformly around the reactor 1, The catalyst feed inlet 9 evenly distributed in the lower part of the reactor 1 and the middle part of the front and rear sides, the screw propeller 12 is arranged on the upper part of one end of the horizontal reactor 1, which can push the liquid flow to move laterally in the direction of the discharge port 3; The screw propeller 12 is only at the inner end of the reactor 1, and the first motor 7 is connected to the outer end of the reactor 1. The first motor 7 is an adjustable speed motor, and its power is only 55-110kw; 1 The top of the other end is provided with a discharge port 3, and the top of the reactor 1 is provided with a manhole 13, which is co...

Embodiment 3

[0026] Embodiment 3, with reference to Figure 5 , Figure 6 , a horizontal polymerization reactor for synthesizing ethylene-propylene rubber, which mainly includes a reactor 1, which can be horizontally placed in the frame of the production device, and multiple groups of heaters uniformly arranged around the reactor 1 Tube bundle 4; the screw propeller 12 is arranged on one end of the horizontal reactor 1, which can push the liquid flow to move laterally toward the discharge port 3; the screw propeller 12 is only at the inner end of the reactor 1 , and the first motor 7 is connected to the outer end of the reactor 1, the first motor 7 is an adjustable speed motor, and its power is only 55-110kw; the top of the other end of the reactor 1 is provided with a discharge port 3, and the reaction A manhole 13 is set on the top of the device 1, which is convenient for operation and maintenance;

[0027] Several feeding ports 9 on the cylinder body of the reactor 1 are evenly distri...

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Abstract

The invention discloses a polymer reactor for synthesizing rubber, which mainly comprises a reactor, wherein a plurality of groups of condensing or heating pipe bundles are uniformly arranged around the inside of the reactor, a plurality of feeding holes are uniformly distributed in the radial direction and the height direction of a reaction cylinder body, the bottom of the reactor is provided with a helical propeller, the helical propeller is connected with a first motor at the outer end of the reactor, the feeding holes are provided with catalyst feeding pipes and blade type stirrers, and connecting shafts of the blade stirrers are connected with a second motor at the outer end of the reactor. The helical propeller and the catalyst feeding pipes are covered with fluorine coatings using polytetrafluoroethylene matrix resin on partial surface in the reactor, the inner circumferential surface of the reactor, the inner circumferential surface of a discharging pipeline and the outer circumferential surfaces of the condensing or heating pipe bundles. An axial flow wiper heat radiating stirring blade of a length penetrating an agitated reactor in the original polymerization agitated reactor is replaced with a short helical propeller to ensure that the stirring power reaching up to 315kw is reduced to about 100-175kw / h, thus the electric energy is saved by above 40 percent.

Description

technical field [0001] The invention relates to a polymerization reactor for synthetic rubber, in particular to a polymerization reactor for synthesizing butyl rubber and ethylene-propylene rubber. Background technique [0002] The polymerization temperature of butyl rubber has a great influence on the copolymerization reaction of isobutylene and isoprene. High temperature will reduce the relative molecular weight of the polymer and reduce the physical and mechanical properties of the resulting rubber. Therefore, in order to obtain polymers with high commercial value, the polymerization temperature must be controlled below -100°C. The characteristic of the butyl rubber production process of the existing slurry method is that the polymerization reactor is a tank reactor. There are multiple groups of condenser tube bundles arranged around the reactor, and the bottom of the reactor center is equipped with an axial-flow scraper heat dissipation stirring paddle, which plays ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J8/10
Inventor 宋晓轩陈文国王社宁李芳学袁自强廖志英刘军杰董晓玲刘应财邵小伟杨鑫
Owner 宋晓轩
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