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Mass detection method of Kesuting syrup

A detection method and technology of cough rate, which are applied in the directions of measuring devices, instruments, scientific instruments, etc., can solve the problem of effective control of morphine content without poppy husk, poor TLC identification effect of Lucky Grass and Morus alba, which is unfavorable for manufacturers and supervision. The control of the product quality of the department has achieved the effect of increasing the ephedra content limit, which is conducive to monitoring and improving the quality monitoring level.

Active Publication Date: 2011-10-26
GUIZHOU BAILING GRP PARMACEUTIAL CO LTD
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AI Technical Summary

Problems solved by technology

In the existing quality standards for Kesuting syrup, the TLC identification effect of Jixiangcao and Morus alba is not very obvious, and the standard for ephedra content is low
In addition, the morphine content in poppy shells has not been effectively controlled
The above problems are not conducive to the control of product quality by manufacturers and supervisory departments

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0025] The detection method of this Kesuting syrup is calculated according to the weight. The Kesuting syrup is made of 200g Jixiangcao, 180g Polygonatum, 150g Baiweiginseng, 150g Bellflower, 100g Saxifrage, 150g Loquat Leaf, 80g Ephedra, 80g Morus Alba, and 50g Poppy Shell. Make 1000ml syrup; This detection method comprises the following steps:

[0026] Properties: This product is brownish-red to brown viscous liquid; fragrant and sweet.

[0027] Identification: (1) Take 20ml of this product, add 50ml of ethanol, mix well, let it stand for 20 minutes, filter, take the filtrate and steam until it has no alcohol smell, add 15ml of water to dissolve, transfer to a conical flask, add 8ml of hydrochloric acid, Heat to reflux for 2.5 hours, place to room temperature, filter, shake the filtrate with chloroform twice, 20ml each time, combine the chloroform solution, evaporate to near dryness, add 1ml methanol to the residue to dissolve, and use it as the test solution. Take another ...

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PUM

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Abstract

The invention discloses a mass detection method of Kesuting syrup, which improves TLC identification to white mulberry root-bark and pink reineckea herb on the basis of the existing quality standard, increases the content limitation of morphine in poppy shell, and enhances the content limitation of ephedra herb, thus leading the level of monitoring the quality of Kesuting syrup to be greatly improved. The application of the mass detection method not only is more beneficial to the monitoring on products by manufacturers and regulatory authorities, but also provides better guarantee for treatment of medical authorities and patients.

Description

technical field [0001] The invention belongs to the technical field of pharmacy, and relates to a detection method of a syrup, in particular to a detection method of a syrup (common name or drug name Kesuting Syrup) for treating cough. Background technique [0002] Kesuting Syrup has the functions of invigorating qi and nourishing yin, nourishing the lungs and relieving cough, benefiting the stomach and promoting body fluid. For colds and acute and chronic bronchitis caused by cough, dry throat, expectoration, asthma embolism. Auspicious grass, Platycodon grandiflorum, Morus alba, Ephedra and poppy shell are the characteristic index components of Kesuting syrup. In the existing quality standards for Kesuting syrup, the TLC identification effect of Jixiangcao and Morus alba is not very obvious, and the standard for ephedra content is low. In addition, the morphine content in poppy shells has not been effectively controlled. The above problems are not conducive to the contr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90
Inventor 孙晓军王晓冬吴春玲郑周琴
Owner GUIZHOU BAILING GRP PARMACEUTIAL CO LTD
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